High-wear-resistance rubber-based composite material and preparation method thereof

A composite material and rubber-based technology, applied in the field of polymer composite materials, can solve the problems of composite materials such as stretching, tearing and wear resistance, so as to improve chemical bonding ability, improve mechanical properties and wear resistance, Strong tear resistance effect

Pending Publication Date: 2022-05-06
QINGDAO UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these methods often lose sight of the performance of c

Method used

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  • High-wear-resistance rubber-based composite material and preparation method thereof
  • High-wear-resistance rubber-based composite material and preparation method thereof
  • High-wear-resistance rubber-based composite material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] 1. Preparation of aramid pulp treated with ionic liquid ethanol solution

[0054] (1) Add 1-propenyl-3-vinylimidazolium chloride salt (structure as follows) ionic liquid into ethanol, and after fully dissolving, obtain a concentration of 0.222g / L ionic liquid ethanol solution;

[0055] (2) Soak the aramid pulp in the ethanol solution of the ionic liquid, the mass ratio of the ionic liquid to the aramid pulp is 1:100;

[0056] (3) drying the soaked aramid pulp;

[0057]

[0058] 2. Preparation of high wear-resistant rubber composites

[0059](1) 100 parts of nitrile rubber, 5 parts of zinc oxide, 1 part of stearic acid, 1.2 parts of 2,2,4-trimethyl-1,2-dihydroquinoline polymer (TMQ), carbon black N550 40 parts, 10 parts of dioctyl phthalate (DOP), 15 parts of aramid pulp treated with ionic liquid of 1-propenyl-3-vinylimidazolium chloride salt in internal mixer with 90°C as the initial temperature Mixed for 7 minutes to obtain the primary product.

[0060] (2) Add ...

Embodiment 2

[0063] 1. Preparation of aramid pulp treated with ionic liquid ethanol solution

[0064] (1) Add 1-propenyl-3-vinylimidazolium chloride salt (structure as follows) ionic liquid into ethanol, and after fully dissolving, obtain a concentration of 0.222g / L ionic liquid ethanol solution;

[0065] (2) Soak the aramid pulp in the ethanol solution of the ionic liquid, the mass ratio of the ionic liquid to the aramid pulp is 1:100;

[0066] (3) drying the soaked aramid pulp;

[0067]

[0068] 2. Preparation of high wear-resistant rubber composites

[0069] (1) 100 parts of nitrile rubber, 5 parts of zinc oxide, 1 part of stearic acid, 1.2 parts of 2,2,4-trimethyl-1,2-dihydroquinoline polymer (TMQ), carbon black N550 40 parts, 10 parts of dioctyl phthalate (DOP), 10 parts of aramid pulp treated with 1-propenyl-3-vinylimidazolium chloride salt ionic liquid in the internal mixer with 90 ℃ as the initial temperature Mixed for 7 minutes to obtain the primary product.

[0070] (2) Ad...

Embodiment 3

[0073] 1. Preparation of aramid pulp treated with ionic liquid ethanol solution

[0074] (1) 1-allyl-3-methylimidazolium chloride salt (structure is as follows) ionic liquid is added in ethanol, obtain concentration after fully dissolving and be 0.206g / L ionic liquid ethanol solution;

[0075] (2) Soak the aramid pulp in the ethanol solution of the ionic liquid, the mass ratio of the ionic liquid to the aramid pulp is 1:100;

[0076] (3) drying the soaked aramid pulp;

[0077]

[0078] 2. Preparation of high wear-resistant rubber composites

[0079] (1) 100 parts of nitrile rubber, 5 parts of zinc oxide, 1 part of stearic acid, 1.2 parts of 2,2,4-trimethyl-1,2-dihydroquinoline polymer (TMQ), carbon black N550 40 parts, 10 parts of dioctyl phthalate (DOP), 15 parts of aramid pulp treated with 1-allyl-3-methylimidazolium chloride salt ionic liquid in the internal mixer at 90 ° C as the initial The temperature was mixed for 7 minutes to obtain the primary product.

[0080]...

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Abstract

The invention discloses a high-wear-resistance rubber-based composite material and a preparation method thereof, and belongs to the field of polymer composite materials. The composite material provided by the invention comprises the following raw materials in parts by weight: 100 parts of rubber, 2-12 parts of an active agent, 0.5-2 parts of an anti-aging agent, 20-70 parts of carbon black, 1-20 parts of a plasticizer, 0.5-2 parts of a vulcanizing agent, 0.5-2 parts of an accelerant and 1-50 parts of aramid fiber treated by an ionic liquid ethanol solution. According to the high-wear-resistance rubber-based composite material prepared by the invention, the aramid fiber and the rubber base are treated by using the ionic liquid, so that the adhesiveness is remarkably improved, and the tear resistance and the wear resistance of the composite material are remarkably improved.

Description

technical field [0001] The invention relates to the technical field of polymer composite materials, in particular to a bonding method for high wear-resistant rubber-based composite materials. Background technique [0002] With the development of rubber industry technology, higher and higher requirements are put forward for the performance of rubber materials. Introducing high-performance fibers, such as aramid fiber, into rubber matrix to prepare composite materials has become one of the hotspots in research and application. At present, aramid / rubber composite materials are widely used in tires, conveyor belts, seals and wipers and other fields. These products all put forward higher requirements on the mechanical properties and tribological properties of materials. Better mechanical / tribological properties are of great significance to prolonging the service life of products, ensuring product safety and reducing energy consumption. However, aramid fiber / rubber composites a...

Claims

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Application Information

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IPC IPC(8): C08L9/02C08L77/10C08L7/00C08L15/00C08L9/06C08L11/00C08K3/22C08K5/09C08K3/04
CPCC08L9/02C08L7/00C08L15/005C08L9/06C08L11/00C08K2003/2296C08L2205/16C08L77/10C08K3/22C08K5/09C08K3/04Y02P20/54
Inventor 李卓张瑞苑欣娜张百慧刘桂志
Owner QINGDAO UNIV OF SCI & TECH
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