A special sizing agent for polyamide material reinforced basalt fiber and its preparation method
A basalt fiber and sizing technology, which is applied in the field of polyamide material reinforced basalt fiber special sizing agent and its preparation, can solve the problems that the compatibility between basalt fiber and polyamide materials cannot be improved, so as to promote wide application and improve compatibility properties, and the effect of improving chemical bonding ability
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Embodiment 1
[0028] (1) Dissolve 15 parts by weight of a modifier containing sodium nitrate: sodium hydroxide: methyldiethoxysilane quaternary ammonium salt in a mass ratio of 3:2:2 with 20 parts by weight of water to form a mixed solution A; 50 parts by weight of polyurethane is dissolved with 20 parts by weight of water, and then 10 parts by weight of silane coupling agent and methyl stearate of 3 parts by weight are added to form mixed solution B;
[0029] (2) Add the mixed solution A obtained in step 1 into the mixed solution B and mix evenly to form a mixed solution C;
[0030] (3) Defoaming the mixed solution C obtained in step 2 to obtain a special sizing for polyamide material reinforced basalt fiber.
Embodiment 2
[0032] (1) Dissolve 10 parts by weight of a modifier containing potassium nitrate: potassium hydroxide: polysiloxane quaternary ammonium salt in a mass ratio of 2:1:1 with 10 parts by weight of water to form a mixed solution A; After 60 parts by weight of polyurethane are dissolved in 30 parts by weight of water, 15 parts by weight of silane coupling agent and 1 part by weight of methyl stearate are added to form mixed solution B;
[0033] (2) Add the mixed solution A obtained in step 1 into the mixed solution B and mix evenly to form a mixed solution C;
[0034] (3) Defoaming the mixed solution C obtained in step 2 to obtain a special sizing for polyamide material reinforced basalt fiber.
Embodiment 3
[0036] (1) Dissolve 20 parts by weight of a modifier containing ammonium nitrate: calcium hydroxide: trialkoxysilane quaternary ammonium salt in a mass ratio of 4:3:4 with 20 parts by weight of water to form a mixed solution A; After 40 parts by weight of polyurethane are dissolved in 30 parts by weight of water, 5 parts by weight of silane coupling agent and 5 parts by weight of methyl stearate are added to form mixed solution B;
[0037](2) Add the mixed solution A obtained in step 1 into the mixed solution B and mix evenly to form a mixed solution C;
[0038] (3) Defoaming the mixed solution C obtained in step 2 to obtain a special sizing for polyamide material reinforced basalt fiber.
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