UV finish paint as well as preparation method and application thereof
A topcoat and epoxy modification technology, applied in the field of coatings, can solve problems such as uneven curing of UV topcoats, photoinitiator migration, etc., to prevent outward migration, good light curing effect, wear resistance and adhesion excellent effect
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[0045] Preparation of epoxy-modified acrylate (E1):
[0046] (S.1) Under nitrogen protection, dissolve 2.08g (10mmol) tetraethoxysilane in 50ml toluene, add 3.76g (40mmol) dimethylchlorosilane and 0.5g ferric chloride to it, at 55°C After reacting for 8 hours, add 2 g of activated carbon therein, stir for 1 hour, and filter to evaporate the toluene in the filtrate to obtain the intermediate product A.
[0047] (S.2) Under nitrogen protection, take 3.28g (10mmol) of intermediate product A and dissolve it in 50ml of toluene, add 10mg of tris(pentafluorophenyl)borane, 0.43g (2mmol) of 4,4'-dihydroxydiphenyl Methanone and 7.65g (38mmol) polyethylene glycol 200, reacted at 35°C for 30min, then raised the temperature to 45°C, continued to mix and react for 3h, added 1g of activated carbon to it after the reaction, stirred and adsorbed for 30min, filtered, and distilled off the filtrate toluene to obtain the prepolymer B whose end group is hydroxyl.
[0048](S.3) Under the protecti...
Embodiment 1
[0082] A UV topcoat, including 40 parts of epoxy-modified acrylate E2, 40 parts of light-curing diluent isobornyl acrylate, 3 parts of antioxidant TPP, and 0.5 parts of leveling agent (BYK-327).
Embodiment 2
[0084] A UV topcoat, including 50 parts of epoxy-modified acrylate E2, 40 parts of light-curing diluent isobornyl acrylate, 3 parts of antioxidant TPP, and 0.5 parts of leveling agent (BYK-327).
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