Heat conduction material as well as preparation method and application thereof
A technology of thermally conductive materials and raw materials, applied in the direction of non-polymer adhesive additives, adhesive types, adhesives, etc., can solve the problem of poor thermal conductivity, inability to meet high thermal conductivity potting adhesives, and potting of electronic components. Glue and other issues
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Embodiment 1
[0079] In this embodiment, a thermally conductive material is prepared, and the specific process is as follows:
[0080] S1. Mix 20g of modified carbon nanotubes and 25g of silicon powder in a ball mill jar; the ball mill jar contains grinding beads of zirconia, wherein the grinding beads with a diameter of 0.8mm are 90g and the grinding beads with a diameter of 4mm are 360g;
[0081] S2. add 0.42g ethylene glycol to the mixture obtained in step S1;
[0082] S3. after the mixture obtained in step S2 is ball-milled for 5h at a rotating speed of 800rpm, the grinding beads are screened out;
[0083] S4. Heat treatment of the mixture obtained in step S3 at 300° C. for 3.5 h.
[0084] The preparation process of this embodiment is all carried out under the protection of nitrogen.
Embodiment 2
[0086] A thermally conductive material is prepared in this example, and the difference between the specific process and Example 1 is:
[0087] Without performing step S4, the mixture obtained in step S3 was directly vacuum-dried at 60°C.
Embodiment 3
[0089] A thermally conductive material is prepared in this example, and the difference between the specific process and Example 1 is:
[0090] Only steps S1 and S3 are carried out, that is, no grinding aid ethylene glycol is added, and no calcination treatment of step S4 is carried out.
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Abstract
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