Surface nickel-phosphorus plated graphene reinforced titanium-based composite material and preparation method thereof
A titanium-based composite material and a technology for the composite material are applied in the field of surface nickel-phosphorus graphene reinforced titanium-based composite materials and their preparation, which can solve the problems of damage, unfavorable composite material properties, poor graphene dispersion effect, etc., and achieve improved performance. , Guaranteed performance, uniform distribution effect
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Embodiment 1
[0047] The ultrasonic power in this embodiment is all 100W, including the following steps:
[0048] S1: Sensitization of graphene
[0049] 0.25g graphene was placed in 250mL deionized water and ultrasonically dispersed for 30min to obtain a graphene suspension, and then 250mL of tin chloride solution (SnCl) was added. 2 10g / L, HCl 40ml / L) continued ultrasonic treatment for 40min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and obtained sensitized graphene.
[0050] S2: Activation of graphene
[0051] The sensitized graphene obtained in step S1 was placed in 250 mL of deionized water and ultrasonically dispersed for 30 min to obtain a sensitized graphene suspension, and 250 mL of palladium chloride solution (PdCl) was added. 2 10g / L, HCl 25ml / L) and ultrasonically treated for 40min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and activated graphene was obtained.
[0052] S3: Nickel-...
Embodiment 2
[0059] The ultrasonic power in this embodiment is all 100W, including the following steps:
[0060] S1: Sensitization of graphene
[0061] 0.5g graphene was placed in 250mL deionized water and ultrasonically dispersed for 60min to obtain a graphene suspension, and then 250mL of tin chloride solution (SnCl) was added. 2 10g / L, HCl 40ml / L) continued ultrasonic treatment for 30min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and obtained sensitized graphene.
[0062] S2: Activation of graphene
[0063] The sensitized graphene obtained in step S1 was placed in 250 mL of deionized water and ultrasonically dispersed for 60 min to obtain a sensitized graphene suspension, and 250 mL of palladium chloride solution (PdCl) was added. 2 10g / L, HCl 25ml / L) and ultrasonically treated for 30min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and activated graphene was obtained.
[0064] S3: Nickel...
Embodiment 3
[0071] The ultrasonic power in this embodiment is all 100W, including the following steps:
[0072] S1: Sensitization of graphene
[0073] 0.75g graphene was placed in 250mL deionized water and ultrasonically dispersed for 60min to obtain a graphene suspension, and then 250mL tin chloride solution (SnCl) was added. 2 10g / L, HCl 40ml / L) continued ultrasonic treatment for 30min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and obtained sensitized graphene.
[0074] S2: Activation of graphene
[0075] The sensitized graphene obtained in step S1 was placed in 250 mL of deionized water and ultrasonically dispersed for 60 min to obtain a sensitized graphene suspension, and 250 mL of palladium chloride solution (PdCl) was added. 2 10g / L, HCl 25ml / L) and ultrasonically treated for 30min, then filtered, rinsed with deionized water until the pH value of the material was neutral, and activated graphene was obtained.
[0076] S3: Nickel-p...
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