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Large-size difficult-to-deform nickel-based superalloy cast ingot and preparation method thereof

A nickel-based superalloy and superalloy technology, applied in the field of superalloys, can solve the problems of high cost, easy cracking, complex process, etc., and achieve the effects of stable mass production, reducing cracking tendency, and eliminating dendrite segregation.

Pending Publication Date: 2022-06-24
BEIJING CISRI GAONA TECH +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the small size of the consumable ingot, it is necessary to prepare large-size bars and large-size disc forgings. There have always been complex processes, easy cracking, high dendrite segregation, more impurities, and high costs, which have affected the popularization and application of this alloy.

Method used

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  • Large-size difficult-to-deform nickel-based superalloy cast ingot and preparation method thereof
  • Large-size difficult-to-deform nickel-based superalloy cast ingot and preparation method thereof
  • Large-size difficult-to-deform nickel-based superalloy cast ingot and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0056] The preparation method of the large-scale hard-to-deform nickel-based superalloy ingot provided in this application includes the following steps:

[0057] Triple smelting: The superalloy raw materials are smelted through the triple process of vacuum induction melting, protective atmosphere electroslag remelting and vacuum consumable remelting to obtain consumable ingots. The raw materials of superalloys can be selected from electrolytic nickel, metal chromium, cobalt plates, and molybdenum bars , electrolytic aluminum block, titanium sponge, high-purity carbon, nickel-magnesium, nickel-niobium, etc.;

[0058] Homogenization treatment: multi-stage homogenization treatment is adopted, the temperature of the consumable ingot is raised to (830-970) ℃ within (2-4) hours, and kept at (830-970) ℃ for (2-4) hours; then ( Raise the temperature to (1115-1125) ℃ at a heating rate of 45-60) ℃ / h, and keep warm for 10-14h; raise the temperature to (1130-1140) ℃ at a heating rate of (...

Embodiment 1

[0063] A method for preparing a large-scale hard-to-deform nickel-based superalloy ingot, comprising the following steps:

[0064] Triple smelting: The raw materials of GH4742 high-temperature and difficult-to-deform nickel-based superalloy are sequentially passed through S1: vacuum induction melting, S2: protective atmosphere electroslag remelting and S3: vacuum consumable remelting to obtain consumable ingots, and vacuum induction melting (VIM ) alloy ingot diameter is 410mm, alloy ingot diameter for protective atmosphere electroslag remelting (P-ESR) is 580mm, and alloy ingot diameter for vacuum consumable remelting (VAR) is 660mm; among them, S1: vacuum induction melting (VIM) operation specifically includes the following steps:

[0065] S1-1. According to the composition requirements of the GH4742 alloy, weigh the raw materials. The weight percentage (wt%) of each raw material is: C: 0.04; Co: 10.0; Cr: 13.0; Mo: 4.5; Ti: 2.50; Al: 2.5; Nb : 2.7; the balance is Ni, put t...

Embodiment 2

[0080] A method for preparing a large-scale hard-to-deform nickel-based superalloy ingot, comprising the following steps:

[0081] Triple smelting: The raw materials of GH4742 high-temperature and difficult-to-deform nickel-based superalloy are sequentially passed through S1: vacuum induction melting, S2: protective atmosphere electroslag remelting and S3: vacuum consumable remelting to obtain consumable ingots, and vacuum induction melting (VIM ) alloy ingot diameter is 390mm, alloy ingot diameter for protective atmosphere electroslag remelting (P-ESR) is 600mm, and alloy ingot diameter for vacuum consumable remelting (VAR) is 660mm; among them, S1: vacuum induction melting (VIM) operation specifically includes the following steps:

[0082] S1-1. According to the composition requirements of the GH4742 alloy, weigh the raw materials. The weight percentage (wt%) of each raw material is: C: 0.05; Co: 10.5; Cr: 13.5; Mo: 5.5; Ti: 2.60; Al: 2.55; Nb : 2.7; the balance is Ni, put ...

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Abstract

The invention discloses a large-size difficult-to-deform nickel-based superalloy cast ingot and a preparation method thereof. The preparation method comprises the following steps: triple smelting: performing triple smelting on a superalloy raw material through vacuum induction smelting, protective atmosphere electroslag remelting and vacuum consumable remelting to obtain a consumable ingot; homogenization treatment: carrying out multi-section homogenization treatment, and carrying out heat preservation on the consumable ingot; raising the temperature and keeping the temperature; raising the temperature and keeping the temperature; and heating, preserving heat and then cooling to obtain the large-size difficult-to-deform nickel-based superalloy cast ingot. The invention further discloses the large-size difficult-to-deform nickel-based superalloy cast ingot prepared by the method. Through the method provided by the invention, the difficult-to-deform nickel-based superalloy with the specification of phi 660 mm can be stably prepared, the prepared alloy ingot is low in segregation, the cracking problem of a large-size ingot is solved, the metallurgical quality of the difficult-to-deform superalloy is improved, the thermoplasticity is high, the later forging cogging cracking is further reduced, and the product quality is improved. And a foundation is laid for preparing large-size bars and large-size disc forgings.

Description

technical field [0001] The application relates to the technical field of high-temperature alloys, and more specifically, it relates to a large-scale hard-to-deform nickel-based superalloy ingot and a preparation method thereof. Background technique [0002] The turbine disk is the key hot end part of the engine, its metallurgical quality and performance level play a decisive role in improving the reliability, safety life and performance of the engine. With the development of high thrust-to-weight / power-to-weight ratio engines, higher requirements are put forward for the temperature bearing capacity, high temperature strength, long life, toughness, fatigue performance, reliability and durability of turbine disks. The degree of alloying of deformed superalloys is getting higher and higher, the content of γ′ phase is getting higher and higher, and the purity is getting higher and higher; at the same time, the diameter of the turbine disk is also increasing, requiring large-scal...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/02C22F1/10C22B9/18C22B9/20C22C19/05
CPCC22C1/023C22F1/10C22B9/18C22B9/20C22C19/056
Inventor 田强秦鹤勇李连鹏张北江丑英玉赵光普杨玉军张文云于腾黄烁杨亮段然齐超李振团宋彬黄瑾刘宁李相材朱洪涛郝永洲刘猛刘军建
Owner BEIJING CISRI GAONA TECH
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