Colouring pigment of eye lense and stained eye lense therewith
A technology for ophthalmic lenses and colorants, applied in glasses/goggles, optics, instruments, etc., can solve problems such as roughness, and achieve the effect of enhanced light resistance
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[0013] Preparation of ophthalmic lens colorants
[0014] First, the method for synthesizing the compound of the coloring agent for ophthalmic lenses represented by the structural formula (1) according to the present invention will be specifically explained.
[0015] First, a compound (carbazole) represented by the following formula (2):
[0016]
[0017] It is mixed with an organic solvent such as methyl ethyl ketone or dioxane, and the mixture is stirred and refluxed at a predetermined temperature in the coexistence of a base.
[0018] When the above mixture is refluxed, the compound represented by the chemical formula (3) is added dropwise to the above mixture, and the reaction is carried out:
[0019] Cl-ROH
[0020] (3)
[0021] Wherein R represents a linear or branched alkylene group having 1 to 5 carbon atoms which may be substituted by Cl or Br. Thus, the compound represented by the following formula (4...
Embodiment 1
[0047] 16 g of carbazole, 14 g of sodium hydroxide and 7 ml of pure water were mixed with 80 ml of methyl ethyl ketone, and the resulting mixture was heated and refluxed for 30 minutes under stirring. While refluxing the resulting mixture, 13 ml of 2-chloroethanol was dropped into it within 1 hour. After the resulting mixture was refluxed for another 3 hours, 8 g of sodium hydroxide was added thereto. While refluxing the mixture, 13 ml of 2-chloroethanol was dropped into it within 1 hour. Then, the resulting mixture was refluxed for 24 hours. The reaction mixture was then left to cool to room temperature, poured into 3 liters of pure water, and extracted with ether. The ether was removed with an evaporator, and the unreacted carbazole was filtered out. From the viscous reaction mixture obtained above, N-(2-hydroxyethyl)carbazole was separated by column chromatography (silica gel / benzene). The yield was 20%.
[0048] Subsequently, 4.5 g of concentrated sulfuric acid was slowly adde...
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