Display device
A display device and phosphor technology, applied in image/graphic display tubes, discharge tubes, screen tubes, etc., can solve problems such as no luminous efficiency, and achieve the effects of improving temperature extinction, reducing damage, and reducing damage to fluorescent films.
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no. 1 Embodiment
[0047] Prepare 9.767g of zinc oxide (ZnO) and yttrium oxide (Y 2 O 3 ) 21.000g, terbium oxide (Tb 4 O 7 ) 2.617g and silicon oxide (SiO 2 ) 12.137g. Mix it well, add a small amount of ethanol to this mixture, and use a graduated pipette in this state to add ytterbium ions (Yb 3+ ) Of aqueous solution. Adjust the ytterbium ion (Yb 3+ ) In the aqueous solution, so that the ytterbium ion (Yb 3+ ) The concentration is 10 mg / ml.
[0048] After the mixture was dried in air at about 120°C for 1 hour, it was placed in an alumina crucible and heat-treated in air at 1400°C for 2 hours. At this time, the alumina crucible is covered with a lid made of alumina (a binder for ceramics is not used). The obtained product was transferred to an agate mortar, pure water was added, and it was sieved while being lightly ground, and then dried in the air at 120°C.
[0049] The rare earth ion obtained in this way: Ytterbium ion (Yb 3+ A plurality of phosphors with different addition amounts of) are respe...
no. 2 Embodiment
[0061] Next, the second embodiment of the present invention will be described. According to the same synthesis method and conditions as the first embodiment, the phosphor base material (ZnY 2 SiO 8 ) Is added with samarium ion (Sm 3+ ) The phosphors are made into multiple test pieces. Next, the luminous intensity was measured in the same evaluation method as in the first example. Table 2 shows that no rare earth ions (Sm 3+ The relative value when the luminous intensity output of the phosphor of) is 1.
[0062] Table 2
[0063] Sm content
(μg / g)
0
(no added)
5
(Comparative example 3)
10
50
100
500
1000
3000
(Comparative Example 4)
Relative brightness
1
0.998
1.000
1.010
1.035
1.012
1.000
0.981
[0064] In addition, the reference numeral 12 in FIG. 1 indicates the additive concentration dependence of the second embodiment ...
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