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Reactive dye composition and method of dyeing with the same

A technology of reactive dyes and compositions, applied in reactive dyes, dyeing methods, azo dyes, etc., can solve problems such as unsatisfactory results

Active Publication Date: 2007-08-15
NIPPON KAYAKU CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to solve the above-mentioned problems, various studies have been carried out (refer to Japanese Patent No. 3168624, for example), but no satisfactory results have been obtained.

Method used

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  • Reactive dye composition and method of dyeing with the same
  • Reactive dye composition and method of dyeing with the same
  • Reactive dye composition and method of dyeing with the same

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] The combinations of reactive dyes and their usage amounts are shown in Table 1.

[0064] In Table 1, C.I.Reactive means Color Index Generic Name.

[0065] Table 1 (combination composition)

[0066] Coordination example 1 (this application invention)

[0067] blue reactive dye

[0068] 0.23 parts of the dyestuff of formula (B)

[0069] 0.13 parts of the dyestuff of formula (5)

[0070] red reactive dye

[0071] 0.11 parts of dyestuffs of formula (7)

[0072] 0.09 part of dyestuff of formula (8)

[0073] yellow reactive dye

[0074] 0.54 parts of the dyestuff of formula (9)

[0075] Coordination example 2 (for comparison)

[0076] blue reactive dye

[0077] C.I.Reactive Blue 221 0.39 parts

[0078] red reactive dye

[0079] C.I.Reactive Red 195 0.20 parts

[0080] yellow reactive dye

[0081] C.I.Reactive Yellow 145 0.59 parts

[0082] Coordination example 3 (for comparison)

[0083] blue reactive dye

[0084] C.I.Reactive Blue 222 0.25 parts

[0085] red ...

Embodiment 2-15

[0128] Adopt the combination of the dyestuff shown in table 3 and the usage amount (part) to replace the combination and the usage amount of the compounding example 1 of embodiment 1, add water in 40 parts of anhydrous sodium sulfate, make total amount respectively and be 980 parts dye bath. 50 parts of cotton knitted fabrics were put into these dyeing baths, and it heated up to 60 degreeC in 20 minutes. After treating at 60°C for 20 minutes, put 20 parts of sodium carbonate and dye at the same temperature for 60 minutes.

[0129] Then, after washing with water and hot water, soaping at 100° C. for 15 minutes in 1,000 parts of an aqueous solution containing the above-mentioned soaping agent, washing with water, and drying to obtain a dyed product.

[0130] table 3

Embodiment 2

[0132] blue reactive dye

[0133] 0.28 parts of the dyestuff of formula (B)

[0134] 0.15 parts of the dyestuff of formula (5)

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Abstract

The invention provides a reactive dye compound and a dyeing method. The compound is provided with dyeing cellulose fiber or fiber material containing cellulose which has good reproducibility, leveling property and color fastness, and has hydrophilicity and well reactivity of dyeing in balance. The reactive dye compound of the invention comprises a blue reactive dye compound of a blue reactive dye shown in a general formula (A) containing a free acid form and a blue reactive dye shown in a general formula (1), and a reactive dye compound containing the blue reactive dye compound, a special red reactive dye and / or a yellow reactive dye. The invention also provides a dyeing method using the cellulose fiber or the fiber material of the compound; in the formula, R represents a hydrogen atom, a halogenous atom or a C1-C4 alkoxyl radical; ml represents an integer form 0 to 2, R1 and R2 respectively and independently represent a hydrogen atom or an alkyl radical which can be substituted; Xl represents a halogenous atom; Y1 represents that -SO2CH is equal to CH2 or SO2CH2CH2Z1 (Z1 represents a radical which breaks away due to the alkaline effect).

Description

technical field [0001] The present invention relates to a reactive dye composition suitable for dyeing cellulose fibers or materials containing cellulose fibers and a dyeing process using the composition. Background technique [0002] Reactive dyes are mostly used in the dyeing of cellulose fibers such as cotton and rayon. It is well known that in the dyeing of cellulose fibers using reactive dyes, it is useful to use yellow, red and blue reactive dyes as dyes for the three primary colors and mix them in various ratios for dyeing. [0003] However, when the affinity, reactivity, dyeing speed, and temperature dependence of each dye used as the dye of the three primary colors are different, there are problems with uniform dyeing such as dyeing spots during dyeing, and color differences between dyeing batches. and other issues such as dyeing reproducibility. With regard to level dyeing and dyeing reproducibility, in recent years, with the diversification of the types and form...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P3/66C09B67/22D06P1/384D06P1/38
CPCC09B67/0045D06P1/38C09B62/006C09B62/008C09B62/09C09B67/0047D06P1/384D06P3/666
Inventor 德山博满漆山武雄宮沢高志小川容一
Owner NIPPON KAYAKU CO LTD