Preparation method of difluoro chloroethane and its production equipment

A technology for difluoromonochloroethane and production equipment, which is applied in the preparation of halogenated hydrocarbons, chemical instruments and methods, organic chemistry, etc., can solve the problems of low conversion rate, low conversion rate and selectivity, low conversion rate and the like, Achieve the effect of satisfying mass production, convenient luminous flux control, and low unit consumption
CN1556083AActive Publication Date: 2004-12-22ZHEJIANG AIKESHENG CHEM

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
ZHEJIANG AIKESHENG CHEM
Publication Date
2004-12-22

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Abstract

A process for preparing difluorochloro ethane from difluoroethane and chlorine gas includes proportionally mixing, three-class photo-chemical reaction while regulating light flux for presenting the high-boiling-point substance peaks with different heights, removing acid, alkali washing, compressing, degassing, rectifying and drying. Its equipment is disclosed also. Its advantages are high conversion rate of difluoroethane and high selectivity and purity of product.
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Description

technical field

[0001] The invention relates to a method for preparing difluoro-chloroethane and its production equipment, in particular to a method for producing difluoro-chloroethane by photochlorination reaction of difluoroethane and chlorine under the action of ultraviolet light Methods. Background technique

[0002] Conventionally utilize difluoroethane under the action of ultraviolet light and chlorine generation photochlorination to produce the method for difluoro-chloroethane to have: 1, the external photochemical reaction method that light source shines into the reactor from the outside of the reactor, like this The reactor is required to have good light transmission and is usually made of glass and quartz glass. Therefore, the reaction equipment is less and is easily damaged during use. At the same time, during the reaction, chlorine gas and some products make the reactor wall form a colored layer. film, which affects the amount of light; 2. There is a light sourc...

Claims

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