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Method for preparing microcrystalline glass/glass carrier material having nano holes in high density

A technology of glass-ceramics and carrier materials, applied in the field of preparation of carrier materials, can solve problems such as low strength and poor size controllability, and achieve the effect of high strength, dense lattice, easy control and mastery

Inactive Publication Date: 2005-01-12
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Using ultra-thin glass as the substrate, the carrier film is prepared on its surface. Due to its low strength and poor size controllability, it has a certain impact on the preparation of biochips and the analysis of samples.

Method used

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  • Method for preparing microcrystalline glass/glass carrier material having nano holes in high density

Examples

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example 1

[0018] Example 1: A method for preparing high-density nanoporous glass-ceramic / glass carrier material, comprising the following steps:

[0019] 1. Preparation of high-density nanoporous glass-ceramic substrate: take the glass-ceramic system as Li 2 O-SiO 2 -Al 2 o 3 -K 2 O-Na 2 O, its weight percentage is respectively 12.0, 78.5, 5.5, 3.0, 1.0; add additive, additive is TiO 2 , AgO, CeO 2 , SnO 2 , Sb 2 o 3 , AuCl, the percentages of each component in the total weight of glass-ceramics and additives are: 0.6, 0.15, 0.015, 0.005, 0.5, 0.0015; each required compound is weighed according to the proportion, and it is prepared after melting and molding at 1490°C Take a sample with a thickness of 0.9mm and a length and width of 25×50mm, and then shield and expose it under a UV lamp with a power of 500w for 15min. The distance between the glass substrate and the light source is 25cm. After heat treatment for 45min, the crystal phase is Li 2 SiO 3 The glass-ceramic, and th...

example 2

[0024] Example 2: if figure 1 Shown, a kind of method for preparing high-density nanoporous glass-ceramic / glass carrier material, comprises the following steps:

[0025] 1. Preparation of high-density nanoporous glass-ceramic substrate: a) Melting of glass: take the glass-ceramic system as Li 2 O-SiO 2 -Al 2 o 3 -K 2 O-Na 2 O, whose weight percent is 11.5Li respectively 2 O, 79.5SiO 2 , 5.3Al 2 o 3 , 2.5K 2 O, 1.2Na 2 O, plus additive, the additive is TiO 2 , AgO, CeO 2 , SnO 2 , Sb 2 o 3 , AuCl, the percentages of each component in the total weight of glass-ceramics and additives are: 0.5TiO 2 , 0.05AgO, 0.035CeO 2 , 0.005SnO 2 , 0.2Sb 2 o 3 , 0.001AuCl; weigh each required compound according to the proportion, melt and mold at 1450°C, and the thickness of the molded sample is 0.5mm; b) UV exposure: shield and expose the molded samples according to the required arrangement , the light source for UV exposure is an ultraviolet lamp, the power is 500w, the e...

example 3

[0028] Example 3: A method for preparing high-density nanoporous glass-ceramic / glass carrier material, comprising the following steps:

[0029] 1. Preparation of high-density nanoporous glass-ceramic substrate: a) Melting of glass: take the glass-ceramic system as Li 2 O-SiO 2 -Al 2 o 3 -K 2 O-Na 2 O, its weight percentage is respectively 12.5, 78.0, 4.5, 3.0, 2.0; add additive, additive is TiO 2 , AgO, CeO 2 , SnO 2 , Sb 2 o 3 , AuCl, the percentages of each component in the total weight of glass ceramics and additives are respectively: 1.0, 0.2, 0.02, 0.005, 0.5, 0.002; after weighing each required compound according to the proportion, melt and shape it at 1550 ° C, The thickness of the molded sample is 1.0mm; b) UV exposure: shield and expose the molded sample according to the required arrangement. The light source for UV exposure is an ultraviolet lamp with a power of 500w and an exposure time of 40min. The distance from the light source is 40cm; c) heat treatmen...

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Abstract

The prodn. steps are: (1) prepn. of high-density nanometrehole microcrystal glass substrate includes glass founding, UV exposuring, crystal coring and crystal grown heating process and acid liquor corroding process; (2) prepn. of nanometrehole glass medium includes glass founding, glass heating process and acid liquor corroding process; (3) nanometrehole glass medium to be carried into microcrystal glass substrate includes that nanometrehole glass medium and gel solution are mixed and high-speed grinded to paste mixture which is squeezed into dense lattice microcrystal glass substrate and drying and burning processes.

Description

technical field [0001] The invention relates to a method for preparing a carrier material that can be used for fixing biological samples, in particular to a method for preparing a high-density nanoporous glass-ceramic / glass carrier material. Background technique [0002] The 21st century is the century of life sciences, and the application of biotechnology in medical diagnosis has gradually matured. At the same time, related biological and chemical device technologies have also been developed rapidly, such as biosensors, bioinformatics, and chemical sensors. However, how to study the functions of so many genes and proteins in the life process has become a common topic for life science workers all over the world, and it is against this background that biochips emerged. [0003] Since the beginning of the 1990s, some countries, mainly the United States, began to develop various biochips. In less than ten years, biochip technology has developed ra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B32/02C03C3/076C03C3/083C03C10/00C03C11/00C03C15/00
CPCC03C10/00C03C15/00C03C11/00C03C3/089
Inventor 韩建军赵修建程金树王田禾刘建党阮健
Owner WUHAN UNIV OF TECH
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