Molybdenum-base alloy and its preparing method
A molybdenum-based alloy and mixture technology, which is applied to the composition field of molybdenum-based alloys, can solve the problems of easy occurrence of cracks, decrease of alloy strength and other properties, influence of intermolecular diffusion, etc., and achieve the effect of improving bonding force
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Embodiment 1
[0018] Embodiment 1, get TiC powder 0.65kg, ZrH 2 Powder 0.15kg, CeC 2 Powder 0.5kg, Y 2 o 3 Powder 0.25kg, C powder 0.2kg, Mo powder 3.5kg, stir evenly with a shovel in a stainless steel pan, sieve, put into a small V-shaped mixer and mix for 90 minutes. Take 44.75kg of Mo powder and the added material after initial mixing, put it in the mixer and mix for 36 hours. The obtained alloy powder is sampled and analyzed at multiple points, and if there is no segregation phenomenon, manual charging is used. Weigh the molybdenum alloy powder and put it into the rubber sleeve of the head product, tamp and seal it, and carry out isostatic pressing. The compression pressure is 200Mpa, and the pressure is maintained for 5 minutes. The pressed parts that pass the density inspection are turned into plug blanks with a certain taper shape. Vacuum intermediate frequency sintering at 2000°C, heat preservation for 3 hours, to obtain molybdenum plug products for piercing and rolling alloy ...
Embodiment 2
[0019] Embodiment 2: get TiH 2 Powder 0.35kg, ZrH 2 Powder 0.1kg, CeC 2 Powder 0.25kg, Y 2 o 3 0.2kg of powder C, 0.1kg of C powder, and 2kg of Mo powder were pre-mixed in the mixer for 80 minutes, and 47kg of Mo powder and pre-mixed additives were taken and mixed in the mixer for 32 hours. After sampling and analysis without segregation, weigh the molybdenum alloy powder and put it into the crucible or the rubber sleeve of the electrode product, and carry out isostatic pressing with a pressing pressure of 180Mpa and hold the pressure for 3 minutes. After turning and compacting the blank, vacuum medium frequency sintering at 1980°C and heat preservation for 4 hours to obtain molybdenum alloy crucible or electrode products.
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