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42 results about "Polonium" patented technology

Polonium is a chemical element with the symbol Po and atomic number 84. A rare and highly radioactive metal with no stable isotopes, polonium is chemically similar to selenium and tellurium, though its metallic character resembles that of its horizontal neighbors in the periodic table: thallium, lead, and bismuth. Due to the short half-life of all its isotopes, its natural occurrence is limited to tiny traces of the fleeting polonium-210 (with a half-life of 138 days) in uranium ores, as it is the penultimate daughter of natural uranium-238. Though slightly longer-lived isotopes exist, they are much more difficult to produce. Today, polonium is usually produced in milligram quantities by the neutron irradiation of bismuth. Due to its intense radioactivity, which results in the radiolysis of chemical bonds and radioactive self-heating, its chemistry has mostly been investigated on the trace scale only.

Method for polonium purification and source preparation in aerosol

The invention belongs to the technical field of radioactive substance impact assessment, and relates to a method for polonium purification and source preparation in aerosol. The method sequentially comprises: (1) transferring a pre-treated polonium sample to be determined into an erlenmeyer flask, and adding <208>Po(IV) or <209>Po(IV) with a certain activity as a tracer to obtain a polonium sampleto be subjected to purification and source preparation; (2) placing the polonium sample obtained in the step (1) in a water bath, evaporating to remove more than 90% of the liquid, and cooling to a room temperature; (3) adding a hydrochloric acid solution, a hydroxylamine hydrochloride solution and ascorbic acid to the sample solution obtained in the step (2), mixing, and uniformly shaking; (4) adding the sample solution obtained in the step (3), and a polished silver sheet or copper sheet to a device capable of providing a certain sealing effect and a certain condensation recovery effect; (5) after installing the device, placing into an oscillator, and carrying out constant temperature water bath oscillation; and (6) after carrying out oscillation for a certain time, taking the poloniumplated silver sheet or copper sheet out of the device, rinsing with distilled water, and carrying out air drying. With the method of the present invention, the recovery rate of the purification and source preparation can be increased and stabilized so as to improve the accuracy of the <210>Po determination result.
Owner:CHINA INST FOR RADIATION PROTECTION

Method for preparing [alpha] measurement source of polonium according to micro precipitation method

The invention belongs to the technical field of radioactive substance measurement, and relates to a method for preparing an [alpha] measurement source of polonium according to a micro precipitation method. The method comprises the steps of (1) adding Te(VI) or Te(IV), a polonium-containing sample, a radioactive tracer <209>Po, a reducing substance and an organic solvent capable of being mixed anddissolved with water and reducing the solubility of TeO2 or elementary substance Te into an aqueous solution so as to enable the Te(VI) or Te(IV) to have an oxidation-reduction reaction with the reducing substance, the TeO2 or elementary substance Te obtained by reduction is enabled to serve as a carrier to take down the radioactive polonium and uniformly disperse the radioactive polonium into theaqueous solution under the effect of the organic solvent; and (2) enabling the carrier taking the radioactive polonium to be uniformly dispersed on a filtering membrane through filtering. Compared with the traditional auto precipitation method for preparing the [alpha] measurement source of the polonium, the method for preparing the [alpha] measurement source for the polonium is short in time, simple to operate, easy to perform batch production, low in cost, higher in acid resistance and anti-interference ability and capable of obtaining a polonium recovery rate (85%-100%) which is close to or higher than that of the auto precipitation method.
Owner:CHINA INST FOR RADIATION PROTECTION

Concentration detection system used for polonium aerosol inside reactor workshop

The invention relates to a concentration detection system used for polonium aerosol inside a reactor workshop. The concentration detection system used for the polonium aerosol inside the reactor workshop is composed of a laser light source (1), an interferometer (2), reactor workshop walls (3), a receiving telescope (4), a photoelectric conversion device (5), corner reflectors (6) and a computer processing system (7). In measurement, lasers sent by the light source are modulated through the interferometer (2) at first, and then are shot into a long-range absorbing light path and reflected and transmitted through a plurality of corner reflectors (6) on the reactor workshop walls (3), and finally are received by the receiving telescope (4), wherein he number of the corner reflectors is determined by the structure of the reactor workshop and the length of the absorbing light path. The photoelectric conversion device (5) converts received optical signals into electrical signals and sends the electrical signals to the computer processing system (7) to generate the Fourier spectrum, and concentration of the polonium aerosol is obtained through calculation. According to the concentration detection system used for the polonium aerosol inside the reactor workshop, rapid and accurate measurement of the polonium aerosol inside the reactor workshop becomes possible, and safety of the inside of the reactor and areas around the reactor is ensured.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Method for polonium leaching in aerosol

The invention relates to the technical field of radioactive substance impact assessment, and relates to a method for polonium leaching in an aerosol. The method sequentially comprises the steps of (1)filtering by a filtering membrane to obtain a tested aerosol sample; (2) adding the filtering membrane, which obtains the tested aerosol sample, into a leaching device; (3) adding <209>Po(IV) with certain activity into the leaching device to serve as a tracer agent; (4) adding hydrochloric acid into the leaching device, enabling the solution to completely immerse the filtering membrane, and theninstalling the leaching device; (5) heating the leaching device so as to enable the solution in the leaching device to be at a slight boiling state, keeping the state, leaching <210>Po on the filtering membrane, and filtering to respectively collect a filtrate and leaching residues; (6) transferring the leaching residues to the leaching device, adding the hydrochloric acid again, then leaching andfiltering by using a method identical to that in the step (5), and carrying out the step for 1-5 times; (7) combining the filtrates of multiple times of leaching; and (8) heating the combined filtrate in a water bath to evaporate more than 90% of the liquid, cooling to obtain a filtrate dry product containing the <210>Po and the tracer agent <209>Po. According to the method, the recovery rate ofpolonium leaching can be improved and stabilized, and thus the accuracy of a <210>Po measurement result is improved.
Owner:CHINA INST FOR RADIATION PROTECTION

Concentration detection system used for polonium aerosol inside reactor workshop

The invention relates to a concentration detection system used for polonium aerosol inside a reactor workshop. The concentration detection system used for the polonium aerosol inside the reactor workshop is composed of a laser light source (1), an interferometer (2), reactor workshop walls (3), a receiving telescope (4), a photoelectric conversion device (5), corner reflectors (6) and a computer processing system (7). In measurement, lasers sent by the light source are modulated through the interferometer (2) at first, and then are shot into a long-range absorbing light path and reflected and transmitted through a plurality of corner reflectors (6) on the reactor workshop walls (3), and finally are received by the receiving telescope (4), wherein he number of the corner reflectors is determined by the structure of the reactor workshop and the length of the absorbing light path. The photoelectric conversion device (5) converts received optical signals into electrical signals and sends the electrical signals to the computer processing system (7) to generate the Fourier spectrum, and concentration of the polonium aerosol is obtained through calculation. According to the concentration detection system used for the polonium aerosol inside the reactor workshop, rapid and accurate measurement of the polonium aerosol inside the reactor workshop becomes possible, and safety of the inside of the reactor and areas around the reactor is ensured.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Method of producing low alpha-ray emitting bismuth, and low alpha-ray emitting bismuth

Provided is low alpha-ray emitting bismuth having an alpha dose of 0.003 cph/cm2 or less. Additionally provided is a method of producing low alpha-ray emitting bismuth, wherein bismuth having an alpha dose of 0.5 cph/cm2 or less is used as a raw material, the raw material bismuth is melted in a nitric acid solution via electrolysis to prepare a bismuth nitrate solution having a bismuth concentration of 5 to 50 g/L and a pH of 0.0 to 0.4, the bismuth nitrate solution is passed through a column filled with ion-exchange resin to eliminate polonium contained in the solution by an ion-exchange resin, and bismuth is recovered by means of electrowinning from the solution that was passed through the ion-exchange resin. Recent semiconductor devices are of high density and high capacity, and therefore are subject to increased risk of soft errors caused by the effects of alpha rays emitted from materials in the vicinity of semiconductor chips. In particular, there is a strong demand for higher purification of solder materials used near semiconductor devices, and there is a demand for low alpha-ray emitting materials. Therefore, the present invention aims to elucidate the phenomenon of alpha ray generation from bismuth, and to provide a low alpha-ray emitting, high-purity bismuth that can be applied to the required materials and a production method thereof, as well as to provide an alloy of low alpha-ray emitting bismuth and tin and a production method thereof.
Owner:JX NIPPON MINING& METALS CORP

Electroplating sampling detection method of 210Po in chemical prospecting sample of mineral exploration by polonium method

The invention belongs to the field of 210Po detection method, and particularly discloses an electroplating sampling detection method of 210Po in a chemical prospecting sample of mineral exploration bya polonium method. The method comprises the following steps: airing or drying a sample in time, grinding until the granularity is less than 417mu m to obtain a specimen, and filling into a bag for later use; weighing the specimen, putting into a beaker, adding ascorbic acid, and adding a hydrochloric acid solution 1#; putting a pre-treated copper sheet into the beaker, and shaking in a constant-temperature shaking bath at 60 DEG C for 110-130 minutes; taking out the sheet after shaking is completed, washing with tap water, and drying the sheet for detecting; measuring the alpha counting ratealpha on the sheet copper surface on a low-background alpha measurement instrument after the sheet is taken off for 30 minutes, and calculating the specific activity of 210Po according to a formula. The method for detecting 210Po in a chemical prospecting sample by adopting an electroplating sampling method has high working efficiency for field mineral exploration, is not influenced by thorium, climate and the like, has a wide detection range, simple analyzing process and easily controlled measurement condition, and is convenient for popularization and application.
Owner:核工业二三0研究所

Twin induced plastic steel with high elongation percentage and high hole expansion rate and manufacture method thereof

ActiveCN102400036BImprove mechanical propertiesAvoid reduction in hole expansion rateNiobiumManganese
The invention provided twin induced plastic steel with a high elongation percentage and a high hole expansion rate and a manufacture method thereof, the steel consists of 0.30 to 0.70 % of carbon, less than or equal to 1.0 % of silicon, 10 to 20% of manganese, less than or equal to 1.0 % of aluminum, 0.005 to 0.20% of polonium, 0.005 to 0.30% of Ra, 0.004 to 0.05% of nitrogen, less than or equal to 0.2% of niobium, less than or equal to 0.3 % of vanadium, less than or equal to 1 of copper and the balance of Fe. The method comprises the following steps of: (1) smelting: smelting by a vacuum furnace, allowing the molten steel to stand for 3-5 min, casting at a casting temperature of 1450-1550 DEG C; (2) hot rolling: heating the casting blank at a temperature of 1150 to 1200 DEG C, with a heating rate of 10-15 DEG C / min, performing heat preservation for 20 to 40 minutes, rolling at an initial rolling temperature of 1150-850 DEG C, stopping rolling at a finishing rolling temperature of 900-600 DEG C, rapidly cooling to room temperature at a rate of more than or equal to 20 DEG C / second after rolling; (3) cold rolling: performing cold rolling with a reduction ratio of the hot rolled plate being 40%-80% ; (4) heat treatment: performing heat treatment at a temperature of 600 to 1000 DEG C, rapidly cooling to room temperature at a rate of more than or equal to 20 DEG C / second after heat preservation for 3 to 10 minutes. The steel of the invention has low cost, a simple method, good quality of the product surface, an excellent processing property and an integrated mechanical property.
Owner:ANGANG STEEL CO LTD
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