This invention discloses a method for extracting
radium from
uranium ore leaching solution, comprising: obtaining a pre-adsorbent material and a main adsorbent material based on macroporous adsorption resin; filling the pre-adsorbent material into a pre-
chromatographic column; filling the main adsorbent material into a main
chromatographic column; connecting the pre-adsorbent column and the main
chromatographic column in series; pumping the
uranium ore leaching solution into the series-connected columns at a preset flow rate; adsorbing
thorium,
radium, and lead elements in the feed solution; eluting the main chromatographic column with
nitric acid solution; eluting the main chromatographic column stepwise with
hydrochloric acid solution; collecting the eluent to obtain a
radium-enriched eluent; and leaving a lead-enriched resin phase on the main chromatographic column. This method utilizes the tandem connection of two columns, acid
gradient elution, and the synergistic coordination effect of
crown ether ionic liquids to enhance the specific recognition and coordination ability of lead ions in the
hydrochloric acid system, improve the selective separation efficiency of radium and lead, reduce usage costs, increase the extraction purity and
recovery rate of radium, and reduce the amount of
radioactive waste generated.