Method for preparing biodiesel from sludge by microwave radiation
A technology of microwave radiation and biodiesel, applied in the field of environmental science, can solve the problems of increasing energy consumption and equipment investment, high viscosity, high content, etc., and achieve the effect of realizing resource utilization, low cost and solving technical problems
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Embodiment 1
[0017] Pre-dry municipal sludge such as activated sludge, digested sludge, industrial sludge such as paint sludge, paper sludge and oily sludge with hot air, add 2% carbon, and put them into a microwave pyrolysis reaction device. Set the power to 2000W, and irradiate at 600-700°C for 22min. Gas, liquid and solid products were obtained respectively, and their product yields are shown in Table 1.
[0018]
[0019] After testing and analysis, it is concluded that the pyrolysis oil obtained from municipal sludge is mainly aliphatic compounds, and the pyrolysis oil obtained from industrial sludge is mainly aromatic compounds with a single ring structure; the gas products are mainly CO and h 2 Mainly.
Embodiment 2
[0021]
[0022] After testing and analysis, it is concluded that the pyrolysis oil obtained from municipal sludge is mainly aliphatic compounds, and the pyrolysis oil obtained from industrial sludge is mainly aromatic compounds with a single ring structure; the gas products are mainly CO and h 2 Mainly, and contains a certain amount of hydrocarbon gas.
Embodiment 3
[0024] Pre-dry municipal sludge such as activated sludge, digested sludge, industrial sludge such as paint sludge, paper sludge and oily sludge with hot air, add 6% silicon carbide, and put them into a microwave pyrolysis reaction device . Set the power to 90kw, and irradiate at 600-700°C for 7 minutes. Gas, liquid and solid products were obtained respectively, and their product yields are shown in Table 3.
[0025]
[0026] After testing and analysis, it is concluded that the pyrolysis oil obtained from municipal sludge is mainly aliphatic compounds, and the pyrolysis oil obtained from industrial sludge is mainly aromatic compounds with a single ring structure; the gas products are mainly CO and h 2 Mainly.
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