Method for producing a catalytic preparation and use of said catalytic preparation
A catalyst and preparation technology, applied in the direction of catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc.
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[0035] Example 1: Production of Stable Titanium-Containing Catalyst Preparations
[0036] 280g of powdered titanium-containing catalyst, with a titanium content of 48.1wt%, and a BET specific surface area of 71.5m 2 / g, average particle size d 50.3 Equal to 2.7 μm, made according to the method described in EP 0736560, by means of a serrated disk dissolving machine (diameter 4cm, speed 1300 minutes -1 ) into 520g of monoethylene glycol and dispersed for 45min. The suspension thus formed was ground in a stirred ball mill (Dispermat SL, 125 mL grinding chamber, 100 mL glass beads, 1 mm diameter) at 3000 rpm for 20 min and at 4000 rpm for 50 min, maintaining the beating cycle. The beads were separated from the suspension and the coarse fraction was separated using a sieve (56 μm mesh). Particle size determination (laser diffraction, Helos) showed an average particle diameter d of 0.92 μm 50.3 , and B 90 / 10= 1.5 μm distribution width. The solids content was about 35% by wei...
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