Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for producing a catalytic preparation and use of said catalytic preparation

A catalyst and preparation technology, applied in the direction of catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc.

Active Publication Date: 2007-01-10
SACHTLEBEN CHEM GMBH
View PDF1 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition to the disadvantage of settling to very densely packed precipitates, which can hardly be settled by stirring, another disadvantage of such systems is that they often contain undesirable auxiliary substances (polymeric wetting and dispersing agents)

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for producing a catalytic preparation and use of said catalytic preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Example 1: Production of Stable Titanium-Containing Catalyst Preparations

[0036] 280g of powdered titanium-containing catalyst, with a titanium content of 48.1wt%, and a BET specific surface area of ​​71.5m 2 / g, average particle size d 50.3 Equal to 2.7 μm, made according to the method described in EP 0736560, by means of a serrated disk dissolving machine (diameter 4cm, speed 1300 minutes -1 ) into 520g of monoethylene glycol and dispersed for 45min. The suspension thus formed was ground in a stirred ball mill (Dispermat SL, 125 mL grinding chamber, 100 mL glass beads, 1 mm diameter) at 3000 rpm for 20 min and at 4000 rpm for 50 min, maintaining the beating cycle. The beads were separated from the suspension and the coarse fraction was separated using a sieve (56 μm mesh). Particle size determination (laser diffraction, Helos) showed an average particle diameter d of 0.92 μm 50.3 , and B 90 / 10= 1.5 μm distribution width. The solids content was about 35% by wei...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
diameteraaaaaaaaaa
Login to View More

Abstract

The invention relates to a method for producing a catalytic preparation, according to which the catalyst, which contains at least one inorganic compound that is solid in normal conditions, is comminuted using a dispersing aggregate into particles with a maximum average particle size d50.3 of 2 mu m, preferably a maximum 1 mu m, conforming to DIN 66141 and 66144 and is then dispersed in a liquid in a concentration of between 1 and 50 wt. %, (in relation to the finished catalytic preparation).

Description

technical field [0001] The present invention relates to a method of producing a catalyst preparation and its use. Background technique [0002] Solid catalysts are often used in the production of polyesters. Such catalysts can be, for example, TiO 2 or by TiO 2 derived compounds. For example, EP 0736560 describes a catalyst comprising an alkali metal titanate or an alkaline earth metal carbonate. [0003] In heterogeneous catalysis, the catalyst is insoluble in the reaction medium but exists as a separate solid phase. In one embodiment concerning such catalysis, the catalyst is maintained as a separate solid phase within the system. In some cases, for example, in the catalysis of an esterification process, the catalyst is added as a powder, but it dissolves during the reaction. Here, a continuous transition from heterogeneous to homogeneous catalysis occurs. [0004] The distribution of the catalyst in the reaction medium greatly affects the reaction progress. [000...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): B01J37/00C09C1/36C01G23/047C09C3/04
CPCC01P2006/12C09C3/041C01P2004/52B01J37/0036C01P2004/62C09C1/3623C01P2004/61
Inventor B·普罗夫特E·希尔施伯格R·奥普特霍斯特尔特J·温克勒K·皮普利斯M·维德勒
Owner SACHTLEBEN CHEM GMBH