High absorbency lyocell fibers and method for producing same

a technology of lyocell fibers and absorbent materials, which is applied in the field of improving the absorbency characteristics of lyocell fibers, can solve the problems of not being able to demonstrate appreciable effects of treatment on the absorbency characteristics of cellulosic materials, and not being able to use lyocell in any significant quantity for these articles, so as to achieve the effect of increasing the absorbency of the material

Inactive Publication Date: 2009-06-18
NGUYEN HIEN VU
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

[0011]This result is obtained in accordance herewith by a hydrothermal treatment, which comprises heating the lyocell fibers in the presence of water at temperatures within the range of up to about 100° C., for a period sufficient to increase the absorbency of the fibers to provide a Syngyna tampon absorbency of at least about 4.4 g / g (at a density of about 0.4 g / cm3) and drying the treated fibers.

Problems solved by technology

Thus, while viscose rayon has seen widespread use in absorbent articles, such as catamenial tampons, sanitary napkins, and other absorbent dressings, lyocell has not been used in any significant quantities for these articles.
Such treatments have not, however, been disclosed as having any appreciable effects on the absorbency characteristics of the cellulosic materials.
None of this literature, however, suggests the use of hot water treatments per se for improving the absorbency of the cellulosic materials thereof.
Again, the cellulosic fibers actually tested in this reference are limited, and the data does not necessarily suggest that the absorbency of lyocell would be improved as significantly as other cellulosic fibers in such a process.

Method used

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  • High absorbency lyocell fibers and method for producing same
  • High absorbency lyocell fibers and method for producing same

Examples

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examples

[0032]The techniques utilized in the hydrothermal treatment of the invention, and the improved absorbency characteristics thus obtained, are illustrated in the following examples, wherein all temperatures are given in degrees Celsius and all parts and percentages are by weight, unless otherwise indicated.

examples 1-4

[0033]Laboratory-made tampons having a mass of about 2.5 g were made according to the general teaching of Friese et al., U.S. Pat. No. 6,310,269, the disclosure of which is hereby incorporated by reference. The tampons were then subjected to the Syngyna Test as described in the US Federal Register, Part III, Department of Health and Human Services, Food and Drug Administration (21 CFR §801.430, Apr. 1, 2001). The results are shown in Table 1, below:

TABLE 1SyngynaSyngynaDensityValue forValueSampleDescription(g / cm3)tampon (g)(g / g)Comparative1.5 denier0.3899.923.89Example 1ATENCEL ®Example 1BTreated10.39011.374.441.5 denierTENCEL ®Comparative2.2 denier0.39410.323.97Example 2ATENCEL ®Example 2BTreated10.31910.965.182.2 denierTENCEL ®Comparative3 denier0.40610.564.14Example 3ATENCEL ®Example 3BTreated1 30.40612.364.82denierTENCEL ®Comparative1.5 denier0.399.973.86Example 4ATENCEL ®Example 4BTreated20.3812.394.801.5 denierTENCEL ®1Hydrothermal treatment in boiling water at 90-100° C. for ...

examples 5 and 6

[0035]Compressed fibrous structures can take advantage of the present invention. The improvements can be shown by use of the Plug Test described hereinbelow.

[0036]Plug Test

[0037]The fiber blend is opened via standard fiber opening and carding equipment.

[0038]Sample Preparation Procedure: A fixed amount of fiber blend, of weight 2 grams, is introduced into a stainless steel mold with a cylindrical cavity (of diameter 1 inch). A cylindrical plunger which fits into the cavity is used to compress the fiber mass. A laboratory press is used to apply the necessary pressure.

[0039]After coming out of the mold the plug is left on the bench for about 20-30 minutes to equilibrate to an equilibrated thickness, from which the density of the plug is calculated.

[0040]Plug Absorbency Test: The test sample is the equilibrated plug. The plug is tested in a Gravimetric Absorbency Tester (as described in Pronoy K. Chatterjee and Hien V. Nguyen, “Mechanism of Liquid Flow and Structure Property Relationsh...

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Abstract

High absorbency lyocell fibers are obtainable by hydrothermal treatment. The fibers can be treated with water at temperatures of at least 60° C. to provide lyocell fibers that can be formed into a random fibrous plug having a mass of 2 g, a density of 0.4 g / cm3, and a diameter of 25 mm which has a GAT Absorbency (at 15 min.) of at least about 3.7 g / g.

Description

CROSS REFERENCE TO RELATED APPLICATIONS[0001]This application is a Divisional application of U.S. Ser. No. 10 / 057,352, filed on Jan. 24, 2002. The complete disclosures of the aforementioned related U.S. patent applications are hereby incorporated herein by reference for all purposes.FIELD OF THE INVENTION[0002]This invention relates to a method for improving the absorbency characteristics of lyocell fibers, and more particularly to such a method which is useful in the preparation of absorbent materials for catamenial tampons, sanitary napkins, and other absorbent dressings.BACKGROUND OF THE INVENTION[0003]There are several forms of rayon manufactured and used in various industries including viscose, cuprammonium, high-wet modulus and lyocell. However, lyocell is distinct from other rayons. For example, the degree of crystallinity of lyocell is at least twice that of rayon; lyocell consists of rather well defined fibrils which can separate due to wet abrasive action, but it is otherw...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): D21C9/00A61F13/20A61L15/28D01F2/00D06M11/05
CPCA61F13/2051A61F13/2085A61L15/28D01F2/00D06M11/05D06M2200/00D06M2101/06C08L1/02
Inventor NGUYEN, HIEN VU
Owner NGUYEN HIEN VU
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