Polymeric material comprising modified lignin
a technology of lignin and polymer, which is applied in the direction of coatings, etc., can solve the problems of miscibility and compatibility with other polymers such as polyolefins, and the disclosure of how the functionalized lignin may be used together with a thermoplastic, and achieves less expensive, environmental protection, and good mechanical properties
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[0096]1. Renol Preparation
[0097]1.1 an Example of how to Prepare Renol of Esterified Lignin—Stearic Acid Esters.
[0098]Full substitution: According to the general procedure of esterification, following amounts were used: Lignin type A2 (1.00 g, 1 eq.), stearic anhydride (6.12 g, 2 eq.), 1-methylimidazole (0.1 ml) and dioxane (15 ml). For purification, celite (50 g) was used with 0.5 M solution of NaHCO3 (400 ml). Some tetrahydrofuran was added to wet the celite. The ester was washed off with neat hexane to give 1.97 g of stearic acid ester as a brown solid.
[0099]Partial substitutions: According to the general procedure of esterification, following amounts were used: Lignin type A2 (1.00 g, 1 eq.), stearic anhydride (0.31 or 0.92 g, 0.1 or 0.3 eq.), 1-methylimidazole (0.1 ml) and dioxane (10 ml). After the reaction the esters were purified according to the general purification of partially substituted esters. 0.1 and 0.3-eq. reactions afforded 1.12 g and 1.01 g respectively of the cor...
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