Dry spinning process of making bright polyacrylic fibre

A bright fiber and dry spinning technology, which is applied in rayon manufacturing, dry spinning, fiber chemical characteristics, etc., can solve the problem of fiber surface smoothness, smoothness decline, unresolved fiber brightness requirements, imperfect parameters, Reasonable and other issues to achieve the effect of improving the finish, reducing voids, and improving gloss

Inactive Publication Date: 2008-12-24
浙江金甬腈纶有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Although our country introduced the production technology of American DuPont Company to produce acrylic fibers by dry method in the mid-1980s, the parameters in the production process are not perfect and reasonable enough, which makes the surface of the fibers severely torn during molding, resulting in smoothness of the fiber surface. , smoothness decreased, so the brightness of the acrylic fiber produced by this method is poor, and it cannot meet the needs of industries such as the production of underwear, clothing and artificial fur, blankets and other industries using acrylic fiber as raw material. Domestic industries still need to rely on imported raw materials for production
[0003] Patent application No. 200410018616.8 "Production method of dry-process acrylic fiber containing vinyl acetate" only studies the raw materials in DuPont's production technology, solves the problem of raw material shortage, finds better substitutes, and effectively reduces the production cost of acrylic fibers. It has improved the spinnability of the fiber and made a significant contribution to the improvement of the dyeing performance of the fiber, but it still has not solved the requirements for the brightness of the fiber, and it cannot meet the needs of various industries that use acrylic fiber as raw material.

Method used

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Experimental program
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Effect test

Embodiment Construction

[0011] The present invention will be further described below in conjunction with the embodiments of the accompanying drawings.

[0012] A preparation of spinning stock solution

[0013] The polyacrylonitrile dry powder PAN and the solvent DMF are fully mixed in a Marco mixer to prepare a spinning solution with a polyacrylonitrile concentration of 33±1%, and an appropriate amount of light coloring agent is added at the same time, and filtered;

[0014] B spinning forming

[0015] The filtrate of the above stock solution is directly pressed into the spinning assembly with a pump, and the stock solution passes through the spinneret holes in the assembly to form a fine stream of the stock solution and enters the spinning tunnel. In the tunnel, the hot nitrogen gas quickly evaporates the solution DMF in the fine stream of the stock solution to make the stock solution The thin stream is solidified to form a silk thread, and the silk bundle is sprayed with cold DMF dilute solvent at...

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PUM

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Abstract

A method for making dry-spun acrylic fiber with large gloss. By improving the original spinning and forming post-treatment process, in the process of washing and drawing, the washing temperature is increased to control at 96°C to 100°C, and the draw ratio control is reduced. At 2.65-4.5 times, reduce the drawing speed to 230-360m / min, and at the same time increase the drying temperature and steam flow in the process of water washing and drying after drawing, which not only ensures that the molecular chain has enough stretching time, but also avoids causing molecular damage. Chain damage, thereby reducing the roughness and damage of the fiber surface, and improving the smoothness and densification of the fiber, making the fiber shiny and bright, which meets the requirements of the domestic fur, clothing and other industries for fiber brightness. It can completely replace imported products.

Description

technical field [0001] The invention relates to a method for producing acrylic fiber by dry method, in particular to a method for producing bright fiber by dry method spinning acrylic fiber. Background technique [0002] Although our country introduced the production technology of American DuPont Company to produce acrylic fibers by dry method in the mid-1980s, the parameters in the production process are not perfect and reasonable enough, which makes the surface of the fibers severely torn during molding, resulting in smoothness of the fiber surface. , smoothness decline, so the brightness of the acrylic fiber produced by this method is poor, and it cannot meet the needs of industries such as producing underwear, clothing and making artificial fur and blankets with acrylic fiber as raw material. Domestic industries still need to rely on imported raw materials for production. [0003] Patent application No. 200410018616.8 "Production method of dry-process acrylic fiber conta...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01D5/04D01F1/02D01F6/18
Inventor 姚家华张宇飞丁国伟邹忠伟张露朝黄志强
Owner 浙江金甬腈纶有限公司
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