Method of separating small hepatocytes by using specific antibody
A technology of hepatocytes and antibodies, applied in the field of efficient separation of proliferative hepatocytes
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Embodiment 1
[0076] Example 1 Preparation of cell fractions rich in small hepatocytes
[0077] Mature rats (8-10 weeks old) were intraperitoneally injected with D-galactosamine (ACROSS) at a concentration of 75mg / 200μl / PBS / 100g body weight. On day 4 after injection, cells were isolated from the liver according to the method of Seglen. Hanks solution supplemented with 0.2 mM EGTA without calcium and magnesium was perfused from the portal vein. After perfusion at a flow rate of 40 ml / min for about 4 minutes, Hanks solution containing 0.02% collagenase (Yakult) was perfused at a flow rate of 20 ml / min for 10 minutes. The hepatocytes were shaken from the digested liver into a beaker according to the prescribed method. Filter the cell suspension with a 250 μm mesh filter and a 70 μm mesh filter, and centrifuge at 50×g for 1 minute. Collect the supernatant and centrifuge at 50 x g for 1 min, repeating 2 times. The supernatant was collected and centrifuged at 50 xg for 5 minutes. The precipi...
Embodiment 2
[0078] Example 2 Expression profile analysis of CD44, D6.1A and BRI3 in small hepatocytes
[0079] The expression profiles of CD44, D6.1A and BRI3 of mature hepatocytes and the mini-hepatocytes prepared in Example 1 were investigated.
[0080] 1) Time-dependent changes in the expression profiles of CD44, D6.1A and BRI3
[0081] Total RNA was prepared from freshly prepared small hepatocytes and small hepatocytes after the initiation of culture, and the expression of CD44 was studied by RT-PCR. GPDH (glycerol-3-phosphate dehydrogenase) was used as a positive control. For the culture of small hepatocytes, the following media were used.
[0082] Dulbecco's Modified Eagle Medium (GIBCO Laboratories)
[0083] +20mM HEPES (Dojindo)
[0084] +25Mm NaHCO 3 (Katayama Chemical Co.)
[0085] +30mg / l Proline (Sigma Chemical Co.)
[0086] +0.5mg / l insulin (Sigma Chemical Co.)
[0087] +10 -7 M Dexamethasone (Sigma Chemical Co.)
[0088]+10% FBS (Hyclo...
Embodiment 3
[0119] Example 3 Isolation of Proliferating Hepatocytes by Anti-CD44 Antibody
[0120] The supernatant obtained by centrifuging at 50×g for 1 minute described in the above i) Preparation method of small hepatocyte-rich cell fraction was collected and centrifuged at 150×g for 5 minutes. The pelleted cells were suspended with the following buffer (phosphate buffered saline (PBS) + 2 mM EDTA (SIGMA Chemical Co.) + 0.5% bovine serum albumin (Serologicals Proteins Inc.)).
[0121] per 1×10 7 Add 80-99 μl of buffer solution to the cells and suspend them, add 1-20 μl of mouse anti-rat CD44 antibody (PharMingene), and incubate at 4-8° C. for 5-10 minutes. Add 10-20 times the volume of buffer, and centrifuge at 300×g for 10 minutes. Suspend the centrifuged pellet with buffer and centrifuge at 300×g for 10 minutes. to each 1 x 10 7 80 μl of buffer was added to the cells to suspend the pellet, and 20 μl of MASC anti-mouse IgG magnetic antibody (Miltenyi Biotec) was added, and incubat...
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