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Nano lamina compound with regular arranged amino radicles

A layered compound and nano-layered technology, applied in the field of nano-layered structure compounds and their preparation, can solve problems such as application limitation, lack of functional layered nano-space environment, and difficulty in functional molecular arrangement.

Inactive Publication Date: 2007-08-29
SHANGHAI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the lack of functional layered nano-space environment and the difficult-to-change layer space structure of the existing layered materials, it is difficult to effectively control the arrangement of functional molecules in the layer space, making the application of these materials limited. very restrictive

Method used

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  • Nano lamina compound with regular arranged amino radicles
  • Nano lamina compound with regular arranged amino radicles
  • Nano lamina compound with regular arranged amino radicles

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0101] p-chloroacetamide phenyl silica layered compound (A), p-3-chloropropanamide phenyl silica layered compound (C), p-4-chlorobutyramide phenyl silica layered compound (E), p- 5-chloropentanamide phenyl silicon oxide layered compound (G), p-chlorobenzamide phenyl silicon oxide layered compound (I), p-chlorophenylacetamide phenyl silicon oxide layered compound (K ) preparation:

[0102] (1) Prepare p-aminophenyl silicon oxide-dodecylsulfate nano-layered compound in advance; its preparation method is: first dissolve the sodium laurylsulfate of 2.88mmol into the deionized water of 250ml, then add 2.74 mmol of p-aminophenyltrimethoxysilane, then slowly drop 0.5nol / L of hydrochloric acid to adjust the pH value of the mixed solution to 2.07, and magnetically stir at room temperature for 12 days to carry out the sol-gel process; finally suction filtration, respectively Washing with deionized water and acetyl, and drying in vacuum to obtain p-aminophenyl silicon oxide-dodecylsulfu...

Embodiment 2

[0105] Chloroacetamidopropyl silica layer compound (B), 3-chloropropionamidopropyl silica layer compound (D), 4-chlorobutyramide propyl silica layer compound (F), 5-chloropentyl oxide layer compound Preparation of amidopropyl silicon oxide layered compound (H), p-chlorobenzamidopropyl silicon oxide layered compound (J), p-chlorophenylacetamidopropyl silicon oxide layered compound (L):

[0106] (1) Prepare aminopropyl silicon oxide-dodecylsulfate nano-layered compound in advance; its preparation method is: first dissolve the sodium laurylsulfate of 2.88mmol into 250ml of deionized water, then add 27.4mmol 3-aminopropyltrimethoxysilane, then slowly dropwise adding 0.5mol / L hydrochloric acid solution to adjust the pH value of the mixed solution to red 2, and magnetic stirring at room temperature for 14 days to carry out the sol-gel process, and finally suction filtration, Washing with deionized water and ethanol respectively, and drying in vacuum to finally obtain aminopropyl sil...

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Abstract

The invention relates to a nanometer layer structure compound and the manufacturing method. It uses 3-amino propyl-3- methoxyl group silicane and amphi-amino benzene 3- methoxy silicane as structure forming material, using the NH2 radical to form layer structure compound under acid condition, and using chloracetyl chloride, 3- chlorine propionyl chloride, 4-chlorine butyric acid chloride, 5-chlorine valeryl chlorine, parachlorobenzoyl chloride, para-chlorobenzene acetyl chloride and the amido and gaining the nanometer layer structure compound with stable and ruled chlorine radical.

Description

technical field [0001] The invention relates to a nano-layer structure compound with regularly arranged chlorine groups and a preparation method thereof, belonging to the technical field of preparation of organic nano-layer compounds. Background technique [0002] As we all know, nanomaterials science is the focus of the future development of materials science, and its research and development have a profound impact on various fields of chemistry. As an important part of nanomaterials, layered nanospace materials such as montmorillonite and hydrotalcite, because they can provide stable two-dimensional nanospace, make them useful in catalytic chemistry, materials chemistry, electrochemistry and biology. Chemistry and other fields are widely studied and applied. In the layered nanospace, functional inorganic or organic molecules can exist in the form of a monolayer, which is impossible to obtain in the macroscopic space, so that it is possible to form composite materials with...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08G77/04C08G77/06C07F7/18
Inventor 姚建施利毅苻英尤晓庆
Owner SHANGHAI UNIV
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