Nano lamina compound with regular arranged amino radicles
A layered compound and nano-layered technology, applied in the field of nano-layered structure compounds and their preparation, can solve problems such as application limitation, lack of functional layered nano-space environment, and difficulty in functional molecular arrangement.
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Embodiment 1
[0101] p-chloroacetamide phenyl silica layered compound (A), p-3-chloropropanamide phenyl silica layered compound (C), p-4-chlorobutyramide phenyl silica layered compound (E), p- 5-chloropentanamide phenyl silicon oxide layered compound (G), p-chlorobenzamide phenyl silicon oxide layered compound (I), p-chlorophenylacetamide phenyl silicon oxide layered compound (K ) preparation:
[0102] (1) Prepare p-aminophenyl silicon oxide-dodecylsulfate nano-layered compound in advance; its preparation method is: first dissolve the sodium laurylsulfate of 2.88mmol into the deionized water of 250ml, then add 2.74 mmol of p-aminophenyltrimethoxysilane, then slowly drop 0.5nol / L of hydrochloric acid to adjust the pH value of the mixed solution to 2.07, and magnetically stir at room temperature for 12 days to carry out the sol-gel process; finally suction filtration, respectively Washing with deionized water and acetyl, and drying in vacuum to obtain p-aminophenyl silicon oxide-dodecylsulfu...
Embodiment 2
[0105] Chloroacetamidopropyl silica layer compound (B), 3-chloropropionamidopropyl silica layer compound (D), 4-chlorobutyramide propyl silica layer compound (F), 5-chloropentyl oxide layer compound Preparation of amidopropyl silicon oxide layered compound (H), p-chlorobenzamidopropyl silicon oxide layered compound (J), p-chlorophenylacetamidopropyl silicon oxide layered compound (L):
[0106] (1) Prepare aminopropyl silicon oxide-dodecylsulfate nano-layered compound in advance; its preparation method is: first dissolve the sodium laurylsulfate of 2.88mmol into 250ml of deionized water, then add 27.4mmol 3-aminopropyltrimethoxysilane, then slowly dropwise adding 0.5mol / L hydrochloric acid solution to adjust the pH value of the mixed solution to red 2, and magnetic stirring at room temperature for 14 days to carry out the sol-gel process, and finally suction filtration, Washing with deionized water and ethanol respectively, and drying in vacuum to finally obtain aminopropyl sil...
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