Propanoic acid polyhexamethylene guanide and preparation method thereof
A technology of polyhexamethyleneguanidine propionate and polyhexamethyleneguanidine, which can be used in botany equipment and methods, chemicals for biological control, animal repellants, etc., and can solve the problem of weak mold killing ability , High hygroscopicity, unable to be made into powdered solids, restrictions and other problems, to achieve excellent bactericidal effect
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[0020] a, synthesis of aminoguanidine propionate
[0021] Add 300 kg of dicyandiamide and 325 kg of ammonium propionate into the rotary mixer and mix for 30 minutes; start heating, stop heating when the temperature rises to 170-180°C, keep the temperature in this range for about 1 hour, and synthesize 440 kg of aminoguanidine propionate;
[0022] b. Polymerization
[0023] Put 400 kilograms of aminoguanidine propionate and 410 kilograms of triethylene propylene diamine into the reaction kettle, add 0.8 kilograms of choline chloride, and follow the predetermined procedure at 100°C (1h)-150°C (2h)-200°C ( 1h) Gradually raise the temperature at -250°C (0.5h), add 0.8 kg of yuntai lactone after the heating process is completed, put it in the reaction kettle, and the reaction is completed to obtain a polyhexamethylene guanidine propionate polymer melt;
[0024] c. Prepare the solution
[0025] Move the polymer melt in the reaction kettle into the hydrolysis tank, add pure water ...
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