Forest grassland fire-proof agent and preparation method thereof
A technology of fire retardant and raw material, applied in fire protection equipment and other directions, can solve problems such as poor fire extinguishing efficiency and fire extinguishing effect, and achieve the effects of good fire prevention effect, simple and fast manufacturing, and good stability.
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Embodiment 1
[0051] 1) Prepare raw materials according to the following weight ratio:
[0052] Demineralized water 30kg
[0053] Phosphoric acid (85% concentration) 20kg
[0054] Urea (content 99%) 15kg
[0055] Catalyst 0.1kg
[0056] Among them, the catalyst is a light yellow-green powder prepared by the Environmental Protection Flame Retardant Technology Center of the School of Materials Science and Technology, Beijing Forestry University. By adding 1 weight part of tin chloride, 2 weight parts of copper sulfate, 1 weight part of sodium chloride, and 1 part by weight, 1 part by weight of aluminum sulfate, 1 part by weight of boric acid and 2 parts by weight of zinc chloride are uniformly ground and mixed.
[0057] In addition, washing powder can be used as the penetrating agent, and acid scarlet 3R can be selected as the coloring agent. The purpose of adding Acid Scarlet 3R to the fire retardant is to mark the location where the fire retardant is sprayed during application, so that ...
Embodiment 2
[0073] 1) Prepare raw materials according to the following weight ratio:
[0074] Demineralized water 23kg
[0075] Phosphoric acid (concentration is 85%) 15kg
[0076] Urea (content 99%) 12kg
[0077] Catalyst: 0.08kg
[0078] The catalyst is the same as in Example 1.
[0079] 2) Take the phosphoric acid in the raw material and add it to the reaction kettle, stir and heat at the same time, control the stirring speed to 50 rpm, and raise the temperature to 50°C;
[0080] 3) Add all the urea in the reactor, and continue to stir the mixture of phosphoric acid and urea at the same time, so that the material is distributed and heated evenly;
[0081] 4) When the temperature rises to 110°C, slowly and evenly add the catalyst into the reaction kettle to make the mixture react;
[0082] 5) Continue heating until the temperature reaches 130°C, control the stirring speed at 60 rpm, observe the reaction phenomenon while heating, as the temperature rises, the light green liquid grad...
Embodiment 3
[0094] 1) Prepare raw materials according to the following weight ratio:
[0095] Demineralized water 41kg
[0096] Phosphoric acid (concentration is 85%) 30kg
[0097] Urea (content 99%) 20kg
[0098] Catalyst: 0.16kg
[0099] Among them, the catalyst is a light yellow-green powder prepared by the Environmental Protection Flame Retardant Technology Center of the School of Materials Science and Technology, Beijing Forestry University. The raw materials include 0.8 parts by weight of tin chloride, 2.5 parts by weight of copper sulfate, 1.2 parts by weight of sodium chloride, ferric chloride 0.8 parts by weight, 0.8 parts by weight of aluminum sulfate, 0.8 parts by weight of boric acid, and 1.5 parts by weight of zinc chloride were uniformly ground and mixed.
[0100] 2) Take the phosphoric acid in the raw material and add it to the reaction kettle, stir and heat at the same time, control the stirring speed to 70 rpm, and raise the temperature to 60°C;
[0101]3) Add urea in...
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