Silicone-acrylate low surface energy ocean anti-fouling paint and preparation method thereof
A low surface energy, marine antifouling technology, applied in the direction of antifouling/underwater coatings, coatings, paints containing biocides, etc., can solve the problems that the service time is difficult to meet industrial requirements, low surface energy, etc., and achieve antifouling Stable effect, high flexibility, long service life effect
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Embodiment 1
[0021] 1) Mix 0.3 part of methyl silicone oil and 0.6 part of di-n-octyl phthalate at 25°C to prepare a coating additive;
[0022] 2) Mix 10 parts of ternary silicon acrylic block copolymer and 2 parts of benzidine yellow at 25°C to prepare a coating additive; mix 10 parts of ternary silicon acrylic block copolymer with 2 parts of benzidine yellow at °C and mix uniformly to prepare a mixture of base material and pigment;
[0023] 3) Add the coating additive obtained in step 1) dropwise to the mixture of coating base material and pigment obtained in step 2) and mix and stir for 1 hour. During the mixing process, the temperature of the mixture is kept at 25° C., and the stirring speed is controlled at 600 rpm / min. The mixture is ready for use;
[0024] 4) The mixture obtained in step 3) was dissolved in 4 parts of butyl acetate (or tetrahydrofuran) solvent to prepare a mixture, and then stirred at 25° C. for 1 hour, and the stirring speed was controlled at 600 rpm / min;
[0025...
Embodiment 2
[0027] 1) Mix 0.4 part of methyl silicone oil and 0.7 part of di-n-octyl phthalate at 27°C to prepare a coating additive;
[0028] 2) Mix 10 parts of ternary silicon acrylic block copolymer and 2.5 parts of benzidine yellow at 27°C to prepare a mixture of paint base material and pigment;
[0029] 3) Add the coating additive obtained in step 1) dropwise to the mixture of coating base material and pigment obtained in step 2) and mix and stir for 1.5 hours. The temperature during the mixing process is kept at 27°C, and the stirring speed is controlled at 500rpm / min. The mixture is ready for use;
[0030] 4) The mixture obtained in step 3) was dissolved in 5 parts of butyl acetate (or tetrahydrofuran) solvent to prepare a mixture, and then stirred at 27° C. for 1 hour, and the stirring speed was controlled at 500 rpm / min;
[0031] 5) After the mixture obtained in step 4) was allowed to stand for 5 hours, the novel marine antifouling paint involved in the present invention was obt...
Embodiment 3
[0033] 1) Mix 0.55 parts of methyl silicone oil and 0.55 parts of di-n-octyl phthalate at 29°C to prepare a coating additive;
[0034] 2) Mix 10 parts of ternary silicon acrylic block copolymer and 3 parts of benzidine yellow at 29°C to prepare a mixture of paint base material and pigment;
[0035] 3) Add the coating additive obtained in step 1) dropwise to the mixture of coating base material and pigment obtained in step 2) and mix and stir for 1 hour. During the mixing process, the temperature of the mixture is kept at 29° C., and the stirring speed is controlled at 600 rpm / min. The mixture is ready for use;
[0036] 4) The mixture obtained in step 3) was dissolved in 4 parts of butyl acetate (or tetrahydrofuran) solvent to prepare a mixture, and then stirred at 29° C. for 1.5 h, and the stirring speed was controlled at 500 rpm / min;
[0037] 5) After the mixture obtained in step 4) was allowed to stand for 4.5 hours, the novel marine antifouling paint involved in the presen...
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