Method for preparing ASA paper-making sizing agent emulsion
A sizing agent and emulsion technology, which is applied in the field of preparation of ASA paper sizing agent emulsion, can solve the problems of unfavorable emulsion storage, low concentration of ASA emulsion, and large amount of particle components added, so as to achieve less dosage and low emulsification cost , High sizing efficiency
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Embodiment 1
[0018] Preparation of emulsifier: 0.75 part of sodium fluoride modified bentonite, 0.1 part of the interlayer anion as Cl - The ionic synthetic hydrotalcite was dispersed in 40 parts of water to prepare an ASA emulsifier, and the solid content of the emulsifier was 2.08%.
[0019] Emulsification of ASA: Weigh 20 parts of the industrial product ASA, add the emulsifier prepared above into the oily ASA, keep the oil-water ratio 1:2, and use high-speed stirring equipment to stir and emulsify at 5000r / min for 5 minutes. The prepared ASA emulsion is a uniform milky white oil-in-water (O / W) emulsion, the pH of the emulsion is 5.31, the viscosity is 0.165 Pa s, the average particle size of the emulsion is 1-3 μm, and the emulsion is centrifuged in a centrifuge (3000r / min) for 10min No change, no phase precipitation, no demulsification phenomenon, and no obvious change in the emulsion after 72 hours.
[0020] In-pulp sizing effect: Take 100 parts of hardwood pulp and disperse in 9900 ...
Embodiment 2
[0022] Preparation of emulsifier: 1.5 parts of sodium fluoride modified bentonite, 0.01 parts of sodium interlayer anion as Cl - Ionic hydrotalcite was dispersed in 40 parts of water to prepare ASA emulsifier, and the solid content of the emulsifier was 7%.
[0023]Emulsification of ASA: Weigh 20 parts of commercial ASA, add the emulsifier prepared above into the oily ASA, keep the oil-water ratio 1:2, and use a high-speed stirring device to shear and emulsify at 8000r / min for 5min. The prepared ASA emulsion is a uniform milky white O / W emulsion, the pH of the emulsion is 4.31, the viscosity is 0.081Pa·s, the average particle size of the emulsion is 1-2.5μm, and the emulsion has no obvious change after 48 hours.
[0024] In-pulp sizing effect: Take 100 parts of hardwood pulp and disperse it in 9900 parts of water. After the dispersion is uniform, add 2 parts of the above-mentioned ASA emulsion and 1 part of Al 2 (SO 4 ) 3 , mixed evenly to form a paper stock, and copied by ...
Embodiment 3
[0026] Preparation of emulsifier: 4 parts of sodium fluoride modified bentonite, 0.02 part of the interlayer anion as Cl - The ionic synthetic hydrotalcite was dispersed in 80 parts of water to prepare ASA emulsifier, and the solid content of the emulsifier was 2.5%.
[0027] Emulsification of ASA: Weigh 20 parts of the industrial product ASA, add the emulsifier prepared above into the oily ASA, keep the oil-water ratio 1:4, and use a high-speed stirring device to emulsify at 10000r / min for 3min. The prepared ASA emulsion is a uniform milky white oil-in-water (O / W) emulsion, the pH of the emulsion is 5.13, the viscosity is 0.265Pa·s, the average particle size of the emulsion is 1-2μm, and the emulsion has no obvious change after 48 hours.
[0028] In-pulp sizing effect: take 100 parts of hardwood pulp and disperse in 9900 parts of water, after the dispersion is uniform, add 3 parts of the above-mentioned ASA emulsion, 1 part of Al 2 (SO 4 ) 3 , mixed evenly to form a paper ...
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