Cathode active material, method of producing the same and nonaqueous electrolyte secondary battery
A positive active material, non-aqueous electrolyte technology, applied in non-aqueous electrolyte batteries, active material electrodes, secondary batteries, etc., can solve the problem of deterioration of charging voltage cycle characteristics, and achieve good charge-discharge cycle characteristics and high energy density. Properties, the effect of inhibiting binding
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Embodiment 1
[0166] First, the manufacturing method of the positive electrode active material used in this specific embodiment is shown below.
[0167] will have an average particle diameter of 13μm and a 0.3m 2 100 parts by weight of lithium cobaltate (average chemical composition analysis value of the specific surface area of / g: Li 1.03 CoO 2.02 ) was dispersed in 3000 parts by weight of an aqueous solution of 2N lithium hydroxide LiOH, and stirred at 80° C. for one hour. 11.15 parts by weight of commercially available reagent nickel nitrate Ni(NO 3 ) 2 ·6H 2 O and 3.67 parts by weight of commercially available reagent manganese nitrate Mn(NO 3 ) 2 ·6H 2 O was dissolved in 100 parts by weight of pure water, and the prepared solution was added to the above dispersion solution for two hours. Moreover, 1.33 parts by weight of commercially available reagent lanthanum nitrate La(NO 3 ) 2 ·6H 2 O was dissolved in 50 parts by weight of pure water, and the prepared solution was add...
Embodiment 2
[0174] A cylindrical secondary battery was manufactured in the same manner as in Example 1, but the amount of nickel nitrate added was changed to 14.87 parts by weight, the amount of manganese nitrate added was changed to 14.67 parts by weight, lanthanum sulfate La 2 (SO 4 ) 3 9H 2 The amount of O was changed to 0.45 parts by weight, and the amount of the lithium hydroxide aqueous solution for adjusting the amount of lithium was changed to 50 parts by weight.
Embodiment 3
[0176] A cylindrical secondary battery was manufactured in the same manner as in Example 1, but with 1.32 parts by weight of cerium nitrate Ce (NO 3 ) 3 ·6H 2 O replaced 1.33 parts by weight of lanthanum nitrate.
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