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Method for identifying abalone origin by atomic absorption spectrum

A technology of atomic absorption spectroscopy and origin, applied in the field of spectral analysis, can solve the problems of inability to identify the origin of abalone and high price

Inactive Publication Date: 2009-05-27
HEBEI UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Therefore, the price of abalone from well-known origins is also higher than that of other origins. At present, there is no detection method to identify the origin of abalone in my country. The existing literature reports on the detection of abalone mainly detect harmful heavy metals, pesticide residues, and limited nutrients. , there is no literature report for the purpose of identifying the origin of abalone, and it is impossible to identify the origin of abalone from the existing data

Method used

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  • Method for identifying abalone origin by atomic absorption spectrum
  • Method for identifying abalone origin by atomic absorption spectrum
  • Method for identifying abalone origin by atomic absorption spectrum

Examples

Experimental program
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Embodiment

[0069] 1. Sample processing:

[0070] Randomly select 100 artificially cultured abalones distributed in the sea area of ​​Qingdao as the standard product of origin, remove the shell, crush the edible part into a slurry with a pulverizer, accurately weigh 1.000-5.000g of the crushed sample, and place it in a 100ml beaker , carry out digestion treatment, add nitric acid into the beaker, the amount of nitric acid added is subject to the sample just submerged, cover the watch glass, and after standing for 10 hours, place the beaker on an electric heating plate for heating and digestion, and the temperature is controlled at 100-200°C Keep the solution slightly boiling for 10 minutes, then add 5-10 ml of hydrogen peroxide, and continue digestion. If the digestion is not complete, remove the beaker from the electric heating plate, add 5 ml of perchloric acid after cooling, and continue digestion on the electric heating plate , digest until the solution in the beaker is nearly dry, co...

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Abstract

The invention provides a method for identifying abalone origin by utilizing atomic absorption spectrometry, comprising the following steps: A. establishing an origin abalone element reference database, that is, using Cultured abalone of Distribution in the same waters as origin standard products, measuring the contents of kalium, sodium, magnesium, calcium, zinc, and iron elements contained in the abalone as data of the element content database of the origin abalone by utilizing atomic absorption spectrometry; B. identifying samples, that is, respectively detecting the abalone samples to be identified with the standard products under the same conditions, so as to obtain the contents of kalium, sodium, magnesium, calcium, zinc, and iron elements contained in the abalone, and identify whether existing significant difference and judge whether the abalone belongs to the origin by comparing statistically the element contents of the standard products and the origin abalone. Because the origin abalone element reference database established in the invention contains wider range, the analysis results by comparing the abalone to be identified and the database is not influenced by subjective sense, thereby providing an objective assessment criteria which has the characteristics of convenience, quickness, simple operation, and high accuracy.

Description

technical field [0001] The invention relates to a method for identifying the origin of abalone by atomic absorption spectroscopy, which belongs to the technical field of spectral analysis. Background technique [0002] Abalone is a single-valve mollusk that crawls on rocks below the low tide line in shallow seas. It is a precious seafood with delicate meat and delicious taste, and is known as the "crown of seafood". Because the aquatic environment of a specific place of origin is closely related to the nutrient composition and content of abalone. Therefore, the price of abalone from well-known origins is also higher than that of other origins. At present, there is no detection method to identify the origin of abalone in my country. The existing literature reports on the detection of abalone mainly detect harmful heavy metals, pesticide residues, and limited nutrients. , there is no literature report for the purpose of identifying the origin of abalone, and it is impossible t...

Claims

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Application Information

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IPC IPC(8): G01N21/31G06F19/00
Inventor 孙建民于丽青孙汉文
Owner HEBEI UNIVERSITY
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