Electrochemical in-situ measurement electrolytic cell device

An in-situ measurement and electrolytic cell technology, which is applied in measuring devices, scientific instruments, and testing wear resistance, can solve the problems of inability to perform electrochemical measurements and unsuitable three-point bending samples, etc., and achieve a simple and practical overall structure, Avoid galvanic corrosion and realize the effect of remaining life

Inactive Publication Date: 2009-06-10
725TH RES INST OF CHINA SHIPBUILDING INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The existing corrosion fatigue technology and its corrosion devices are designed for fatigue samples, but the corrosion fatigue crack growth samples cannot be electrochemically measured using the same corrosion device
At present, there are few reports on electrochemical in-situ measurement techniques for corrosion fatigue crack growth of metal materials, only a brief introduction to corrosion test design in corrosion fatigue tests, such as: Aviation Industry Standard HB 6626-92 "Metal Materials i

Method used

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  • Electrochemical in-situ measurement electrolytic cell device
  • Electrochemical in-situ measurement electrolytic cell device
  • Electrochemical in-situ measurement electrolytic cell device

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Embodiment

[0013] The main structure of this embodiment includes a front cell body 7, a rear cell body 3, a working electrode or a three-point bending sample 1, a bolt 2, a water outlet hole 4, a water inlet hole 5, an auxiliary electrode 6, a salt bridge 8, and a reference electrode 9 and Erlenmeyer flask 10; the front cell 7 and the rear cell 3 are symmetrical half-body structures, and the two are aligned to form the electrolytic cell box of the box-type structure, and the front and rear cells 7 and 3 are connected by long bolts 2 3. It is fixed on both sides of the three-point bending sample 1. There is a gasket at the connection between the two tanks and the sample. The gasket can prevent the leakage of the corrosive liquid; the front tank 7 is divided into a front plate and a left side plate. , the right side plate and the bottom plate, wherein the four top corners of the H-shaped front plate are respectively shaped with round holes for fixing the bolts 2, and the distance between th...

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Abstract

The invention relates to an electrolytic cell device of electrochemistry electrochemistry for performing corrosion fatigue crack propagation experiment on metal materials, belonging to the technical field of material corrosion research, mainly comprising a front trough solid, a rear trough solid, a three point bending specimen, a bolt, a water outlet, a water inlet, an auxiliary electrode, a salt bridge, a reference electrode and a conical flask; the front trough solid and the rear trough solid are symmetrical halfbody structures, which fix the electrolytic cell in a box shaped structure on two sides of the three point bending specimen through a thru bolt. A groove placing auxiliary electrode is arranged at the center of the front plate inner side of the front trough solid. One end of the salt bridge communicates with the auxiliary electrode and the work electrode through etching solution, and the other end is connected with the reference electrode through the conical flask full of saturated potassium chloride solution. A left posterior lateral plate and a right posterior lateral plate have the same height and the same width with a left front lateral plate and a right front lateral plate, which is a symmetrical shape and structure, having simple and practical structure, multiple measurable functions, long service life, high measuring precision and good accuracy.

Description

Technical field: [0001] The invention belongs to the technical field of material corrosion research and relates to an electrolytic cell device capable of performing electrochemical in-situ measurement for corrosion fatigue crack growth tests on various metal materials. Background technique: [0002] Corrosion fatigue refers to the fracture phenomenon of metal materials caused by the synergistic effect of corrosive medium and alternating stress or pulsating stress. In engineering practice, various structures subjected to cyclic loads may be damaged by corrosion fatigue, causing major accidents and bringing heavy losses to the national economy. The development of modern industry requires components to withstand more severe corrosion and load conditions, which makes the problem of corrosion fatigue more serious. In corrosion fatigue damage, its life is mainly controlled by crack propagation behavior, so it is of great significance to study the crack growth law and its influenc...

Claims

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Application Information

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IPC IPC(8): G01N3/56G01N17/02
Inventor 张慧霞程文华邓春龙
Owner 725TH RES INST OF CHINA SHIPBUILDING INDAL CORP
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