Method for producing cigarette flavor by maillard reaction with red date extract as raw material

A technology of jujube extract and Maillard reaction, which is applied in the fields of application, essential oils/spices, tobacco, etc., can solve the problems of long time consumption, few types of spices, and high cost of sugar, so as to improve the quality of tobacco, make the smoke soft and delicate, The effect of increasing the concentration of smoke

Active Publication Date: 2009-08-05
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Some people in China simply react glucose with amino acids to form Maillard reaction products. This kind of spice has few varieties and single aroma, which has limited improvement on the quality of tobacco smoking.
Chinese patent (CN1162008A) discloses "a method for producing tobacco spices". It uses tobacco materials as raw materials. After the raw materials are crushed, they are steamed and sterilized by adding water, and fermented for 2 hours at 20-70°C. ~3 days, followed by solvent extraction, and then separation and purification to obtain the product. This method is complex, time-consuming, and the source of raw materials is unstable.
Chinese patents (CN1415717A and CN1175623A) disclose "the method for producing spices with tobacco extract as raw material" and "the preparation method and utilizat

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039]Weigh 500 grams of jujube extract, put it into a three-necked flask, add 30 grams of alanine, start stirring, then add ammonia water to adjust the pH to 9.7, connect the reflux condenser, heat to 90°C with an oil bath, and keep the temperature constant for 3 hours , the stirring speed is 200 rpm, then stop heating, pour out the reactant, remove insoluble matter with gauze, and the obtained filtrate is the product of the present invention. The resulting product exhibited a strong date, roasted and nutty aroma. The product was added to blank cigarettes in an amount of 0.8‰, and experts were asked to evaluate the smoking. The results are shown in Table 1.

Embodiment 2

[0041] Weigh 500 grams of jujube extract, put it into a three-necked flask, add 15 grams of alanine, 15 grams of proline, start stirring, then add ammonia water to adjust the pH to 9.7, connect the reflux condenser, and heat to 95°C, constant temperature for 3.5 hours, stirring speed at 200 rpm, then stop heating, pour out the reactant, remove insoluble matter with gauze, and the obtained filtrate is the product of the present invention. The obtained product showed a strong jujube aroma and burnt sweet aroma. The product was added to the blank cigarette at an amount of 0.8‰ and asked to be evaluated by tobacco experts. The results are shown in Table 1.

Embodiment 3

[0043] Weigh 500 grams of jujube extract, put it into a three-necked flask, add 40 grams of proline, start stirring, then add 50 grams of propylene glycol, adjust the pH to 9.7 with concentrated ammonia water, connect the reflux condenser, and heat to 110 with an oil bath ℃, constant temperature for 3 hours, stirring speed is 300 rpm, then stop heating, pour out the reactant, remove insoluble matter with gauze, and the obtained filtrate is the product of the present invention. The obtained product exhibits a strong roasting aroma and rice aroma. The product was added to blank cigarettes in an amount of 0.8‰, and experts were asked to evaluate the smoking. The results are shown in Table 1.

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PUM

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Abstract

The invention discloses a method for producing tobacco perfume by adopting red jujube extract through the Maillard reaction, which relates to a preparation method of tobacco perfume. The preparation method comprises the following steps: (1) preparing the red jujube extract; (2) adding one or a plurality of types of aminophenol or amines in the red jujube extract, adding H2O and solvent which are placed in a reaction kettle to be mixed into a homogeneous reaction system, adjusting the pH value of the reaction system, putting reagent into a return pipe, leading the reagent to perform the Maillard reaction under the conditions of mixing, heating and normal pressure, and obtaining the tobacco perfume by the return reaction. The method enables the perfume material in the red jujube extract to mutually serve the perfume material produced in the Maillard reaction, thereby forming the tobacco perfume with rich and special fragrance and multiple type, having strong fruity coordinating with the smoke gas of a cigarette, increasing the smoke gas concentration, leading the smoke gas to be soft and exquisite, hiding the mixed gas and obviously improving the tobacco quality.

Description

technical field [0001] The invention relates to a method for preparing tobacco flavor, in particular to a method for producing tobacco flavor by Maillard reaction using jujube extract as raw material. Background technique [0002] In the prior art, there are generally two types of tobacco flavors used in cigarettes: one is natural extract flavors, using natural components contained in natural flavors or potentially coordinated with smoke; the other is synthetic flavors, using A synthetic fragrance monomer that coordinates with smoke and has a certain effect on smoke. The flavors for tobacco made by these two types of spices alone or by blending are simple in process, but the effect is not very good due to monotonous aroma and single effect on smoke. The research on tobacco flavors in our country has always been relatively backward, and most of the flavors depend on imports. Therefore, it is necessary to develop tobacco flavors with good effects. Reactive spices (i.e. Maill...

Claims

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Application Information

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IPC IPC(8): C11B9/00A24B15/30
Inventor 朱巍殷发强肜霖潘婷婷董世良何佳文佘跃群邵璐
Owner HUBEI CHINA TOBACCO IND
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