Method for preparing flocculating agent for water treatment

A flocculant and water treatment technology, applied in the field of modified water treatment flocculant preparation, can solve the problems of application limitation, non-compliance with environmental protection requirements, and high cost of preparing polymer organic flocculants, and achieve high water solubility and viscosity stability, High water solubility, thickening, and flocculation performance are remarkable

Inactive Publication Date: 2009-09-02
LANZHOU UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Therefore, in recent years, researchers at home and abroad have devoted themselves to the research of high-efficiency, non-polluting, non-toxic polymer flocculants, and the most research results are polymer inorganic flocculants, and the preparation technology has been continuously improved, and some achievements have been successfully applied. And achieved certain economic benefits; microbial flocculants have been gradually studied recently, but they are still in the laboratory research stage; while the preparation cost of polymer organic flocculants is high, the residual monomers are highly toxic, and do not meet environmental protection requirements. Restricted, especially in the field of water supply and wastewater treatment, the application effect is not ideal

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0009] Take by weighing 50g of guar gum powder, simultaneously weigh 24g of monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 60° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.

Embodiment 2

[0011] Take by weighing 50g of guar gum powder, simultaneously weigh 35g of monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 70° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.

Embodiment 3

[0013] Take by weighing 36g of guar gum powder, simultaneously weigh 30g monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 70° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.

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Abstract

The invention discloses a method for preparing a flocculating agent for water treatment, which comprises the following steps of: by weight percent, weighing 40 to 60 percent of guar gum, 20 to 40 percent of chloroacetic acid, and 20 to 35 percent of alkaline catalyst, placing weighed organic acid into a reactor; adding 80 percent of organic solvent till the organic acid dissolves uniformly and adding an excess amount of 30 percent alkaline catalyst; pouring the guar gum into the reactor, and stirring the mixture in the reactor at room temperature for 5 to 30 minutes till the mixture is uniform; after the material is in a semidry state, crushing the material and passing the crushed material through a sieve; placing the material in an reactor, and heating the reactor in a water bath for promoting the reaction, wherein the water bath temperature is kept between 50 and 80 DEG C, and the reaction lasts for 10 to 60 minutes; after reaction, obtaining carboxyl methylated guar gum by grinding and sieving.

Description

technical field [0001] The invention relates to a preparation method of a water treatment flocculant, in particular to a preparation method of a modified water treatment flocculant with adsorption and flocculation functions. Background technique [0002] Coagulation technology is one of the indispensable treatment methods in water supply and sewage treatment. The key to coagulation is the development of high-efficiency flocculants and the development of new flocculation equipment. [0003] At present, the use of flocculants in most water plants in China is still dominated by inorganic flocculants such as ferric chloride, aluminum sulfate, polyaluminum salt (PAC) and polyferric sulfate (PFS). In European countries, polymer flocculants are more commonly used, and the treatment effect is better. After adding the polymer flocculant, the floc sinks faster, the sludge produced is denser, and the dosage is less than that of the inorganic flocculant, so it has better application v...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/52
Inventor 赵霞冯辉霞俞树荣雒和明梁瑞王玉晓
Owner LANZHOU UNIVERSITY OF TECHNOLOGY
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