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Method for regenerating absorbent

A technology of absorbent and membrane module, which is applied in the field of absorbent recycling, can solve problems such as low efficiency, high energy consumption, and cost, and achieve good economic and social benefits, environmental protection, and energy conservation.

Active Publication Date: 2012-11-07
溧阳常大技术转移中心有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Using this process to regenerate 1 cubic meter of absorbent requires 100-200 kilograms of steam, and the energy consumption is quite high
Although a lot of improvements have been made to the structure of the absorption tower, the type of filler and the composition of the absorbent through a large number of industrial practices and laboratory research over the years, the effect is not great.

Method used

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  • Method for regenerating absorbent
  • Method for regenerating absorbent
  • Method for regenerating absorbent

Examples

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Embodiment Construction

[0019] Such as figure 1 As shown, the MDEA waste liquid enters the filter (11) through the pump (12) to filter the feed liquid to be regenerated, and the suspended matter above 0.01mm is filtered out. The filtered feed liquid is measured by the flow meter (10), enters the heat exchanger to be heated to the set temperature, enters the membrane module (1) for membrane distillation separation, and the regenerated feed liquid is measured by the flow meter (2) and then goes to the adsorption tower . The desorbed acid gas is measured by the gas flow meter (6) at the outlet of the tube side of the membrane module, and enters the condenser for condensation and recovery. The vacuum degree of the tube side of the membrane module is controlled by a vacuum pump (7), a vacuum tank (8) and a vacuum pressure transmitter (4).

[0020] In the embodiment of the present invention, the treatment liquid is the rich MDEA absorbent that has been used in the desulfurization process, and the MDEA an...

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Abstract

The invention relates to a rich absorbent regeneration technique for separating gas for absorbent. The technique comprises the following steps: a membrane module is used as unit equipment, and the rich absorbent flows in the shell side of the membrane module; gas penetrating through the membrane enters a pipeline and is pumped by a vacuum pump to a collection tank for recovery; regenerated absorbent is collected into a liquid storing tank for reuse; rich liquid of absorption liquid enters a filter to be filtered for feed liquid regeneration; the filtered feed liquid is measured through a flowmeter and enters a heat exchanger to be heated to a set temperature (30-70 DEG C); the heated liquid enters the membrane module to carry out distilling separation; regenerated feed liquid enters an absorption tower after being measured by the flowmeter; acidic gas generated by desorption is measured by a gas flowmeter at the outlet of the pipeline of the membrane module; and the acidic gas enters a condenser for condensation and recovery. The method provided by the invention can regenerate rich absorbent at the temperature which is 50-100 DEG C lower than a general method, can regenerate absorbent in a temperature range of 30-70 DEG C and saves energy by 50-200 percent compared with a traditional generation method, thereby having favorable economic and social benefits.

Description

technical field [0001] The invention belongs to the technical field of absorbent recovery and utilization, in particular to the rich absorbent regeneration technology for separating gas by absorbent. Background technique [0002] Absorption is an important operation unit of chemical separation engineering. The absorption processes mainly include packed tower method, swirl plate tower method, spray tower method, impact method, etc. The absorbent used for absorption and separation will lose its activity after running for a certain period of time, and it needs to be regenerated or desorbed before it can continue to be used, otherwise it will be thrown away as waste. The current regeneration methods are almost all desorption with high temperature in the re-tower. [0003] Natural gas is a mixture of hydrocarbons and various impurities, including acid gases such as hydrogen sulfide and carbon dioxide. The purification of natural gas is mainly based on the ammonia method. Nearly...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D53/14B01D61/36
Inventor 王树立李贝贝蔡培
Owner 溧阳常大技术转移中心有限公司