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Method for preparing fire retardant modification timber

A modification and flame retardant technology, applied in wood treatment, impregnated wood, manufacturing tools, etc., can solve the problems of flammability of modified wood and easy loss of flame retardants, and achieve flame retardant performance, good water solubility, The effect of improving physical and mechanical properties

Inactive Publication Date: 2009-12-16
EVERFIRST WISEFUND TECH BEIJING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem to be solved by the present invention is to overcome the problem that the flame retardant is easily lost inside the wood, resulting in the flammability of the modified wood, and to provide a new preparation method of the flame retardant modified wood, which can be processed by one-time impregnation. To improve the use performance of wood and excellent flame retardant effect, simplify the process of modified wood, the dimensional stability and mechanical properties of modified wood are significantly improved, and at the same time, it can keep the fire retardant performance of wood for a long time

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] 1. Preparation of flame retardant (by weight): 102 parts of phosphoric acid, 62 parts of urea and 87 parts of water are mixed together and stirred evenly to obtain final product; 2. Preparation of urea-formaldehyde resin preshrunk (by weight) : 560 parts of formaldehyde, 170 parts of urea, 15 parts of melamine and 700 parts of water are mixed together and stirred evenly to obtain final product; 3. After 20 parts by weight of flame retardant are added to 80 parts by weight of urea-formaldehyde resin preshrinkage solution and completely dissolved Obtain the impregnation solution; 4. Impregnation treatment of Paulownia: vacuumize to vacuum degree -0.085Mpa, keep for 15min, use 1.0Mpa in the pressurization stage, keep for 30min; 4h, drying at 103°C for 5h, and drying at 120°C for 1h.

[0022] The flame-retardant modified Paulownia prepared in this example has a final weight gain of 40%, an oxygen index of 70%, a dimensional stability of 20%, a surface hardness of 100%, and ...

Embodiment 2

[0024] The only difference between this embodiment and Example 1 is that the parts by weight of each component of the flame retardant are as follows: 51 parts of phosphoric acid, 56 parts of melamine, and 150 parts of water; other steps and parameters are exactly the same as those of Example 1.

[0025] The flame-retardant modified Paulownia prepared in this example has a final weight gain of 35%, an oxygen index increased by 40%, dimensional stability increased by 13%, surface hardness increased by 85%, and water absorption decreased by 65%.

Embodiment 3

[0027] The only difference between this embodiment and Example 1 is that the parts by weight of each component of the flame retardant are as follows: 118 parts of phosphoric acid, 107 parts of urea, 15 parts of diammonium hydrogen phosphate and 35 parts of water; other steps and parameters are the same as in the embodiment 1 is exactly the same.

[0028] The flame-retardant modified Paulownia prepared in this example has a final weight gain rate of 40%, an oxygen index increase of 75%, a dimensional stability increase of 15%, a surface hardness increase of 90%, and a water absorption rate decrease of 90%.

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PUM

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Abstract

The invention discloses a method for preparing a fire retardant modification timber. The method comprises the following steps of: (1) adding a fire retardant into a urea formaldehyde resin concentrate to obtain a timber impregnation liquid after the fire retardant is completely dissolved; (2) making the impregnation treatment of the timber to be treated by using the vacuum pressure method and the timber impregnation liquid obtained in the step (1); and (3) drying the timber to be treated to obtain the fire retardant modification timber. In the method, the fire retardant is directly added into the urea formaldehyde resin concentrate to form the impregnation liquid, so that by one-time impregnation treatment, the use performance of the timber is improved, the fire retardant effect is enhanced, the process for modifying the timber is simplified, and other steps which are needed after the timber modification to realize the fire retardant function are saved. The method has the advantages of simple process and unnecessary complex equipment; and when the method is adopted to treat the timber, the size stability of the treated timber is obviously improved, the physical and mechanical properties are obviously improved, the weight gain rate of the timber is between 25 and 50 percent, and the oxygen index is increased by 40 to 80 percent.

Description

technical field [0001] The invention relates to a method for modifying wood, in particular to a method for preparing flame-retardant modified wood, and belongs to the field of chemical modification of wood. Background technique [0002] Wood is closely related to people's daily life. Chemical modification of wood is an effective way to improve the natural defects of plantation wood and low-grade wood. The density, surface hardness, wear resistance and dimensional stability of wood after treatment are greatly improved. At present, my country has extensively carried out research on the strengthening technology of fast-growing wood. [0003] As people's requirements for wood quality are getting higher and more comprehensive, multi-functional wood modification technology is also the main direction of wood modification development, not only to improve material properties, but also to make wood have anti-corrosion properties and flame retardant properties. Environmental protectio...

Claims

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Application Information

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IPC IPC(8): B27K3/00B27K3/52B27K3/08B27K5/04
Inventor 雷得定周军浩邓雄飞
Owner EVERFIRST WISEFUND TECH BEIJING
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