Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Cracking agent C9 primary hydrotreated oil deodorising method

A hydrogenation oil and deodorization technology, which is only applied in the direction of multi-stage series refining process, can solve the problems of not meeting the quality requirements of solvent oil, odor, instability, etc., and achieve low cost, good effect, and no new The effect of increasing pollution

Active Publication Date: 2012-07-11
广东新华粤石化集团股份公司
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] After a period of low temperature and low pressure, the primary hydrogenated oil that has been hydrotreated with a high-activity catalyst has a large amount of monocyclic olefins, sulfur, and nitrogen impurities. Although the quality of the oil is improved and the appearance is light, it still has a foul smell. Stable, easy to change color, can not meet the quality requirements of solvent oil

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Cracking agent C9 primary hydrotreated oil deodorising method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0022] In 1000 grams of primary hydrogenated oil, add 2 grams of activator citric acid, stir and dissolve, then add binary solid stable chlorine dioxide that accounts for 0.25% of the weight of primary hydrogenated oil and is made of 4 times the weight of water solution, stirred for 1 hour, settled for 25 minutes and drained the precipitate in the reaction solution; the reaction solution was neutralized to neutrality with alkaline neutralizing agent sodium hydroxide after the precipitate was discharged; then 300 grams of water was added for washing until The oil product is neutral, and it can be obtained after draining clean water. The above steps are all carried out under normal temperature and pressure. It is distilled to obtain the aromatic solvent oil that meets the market demand.

[0023] Comparison of deodorized solvent oil obtained in the present invention with primary hydrogenated oil without deodorization:

[0024]

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a cracking agent C9 primary hydrotreated oil deodorising method and the method comprises the following steps: a. dissolving acidic activator in primary hydrotreated oil; b. using 3-5 times of water to prepare stabilized chlorine dioxide water solution; c. mixing the obtained solutions in step a and step b, stirring for 0.5-3h, precipitating for 0.1-2h, discharging the precipitate in reaction liquid; d. neutralizing the reaction liquid without precipitate with basic neutralizer to ensure the precipitate to be neutral; e. washing with water 1-2 times, discharging water and obtaining the finished product, wherein the content of the acidic activator is not more than 0.4% of the primary hydrotreated oil, the content of stabilized chlorine dioxide is 0.1-0.5% of primary hydrotreated oil and the above steps are performed at room temperature and normal pressure. The invention has simple process, low cost, no new pollution and good effect.

Description

technical field [0001] The invention relates to a refining method of cracked C9, in particular to a deodorization method of cracked refined C9 primary hydrogenated oil. Background technique [0002] Ethylene plant cracks carbon nine, after cutting, the distillation range is in the range of 140-200 ° C, called refined C9, it contains a large amount of naphthenes and aromatics, the sum of the two is as high as 96%, and it is a good solvent oil raw material. However, due to the presence of diolefins, monoolefins and S, N impurities, it produces a foul odor and is unstable in storage. Therefore, most of them are used as fuel oil at present, failing to give full play to its economic value. [0003] The refining of refined carbon nine usually adopts the method of secondary hydrogenation, that is, one-stage hydrogenation to remove dienes, and two-stage hydrogenation to remove mono-olefins and sulfur and nitrogen impurities. [0004] After a period of low temperature and low pres...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10G53/12
Inventor 麦启文谢桂芳庞海舰叶富强穆智宇
Owner 广东新华粤石化集团股份公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com