Method for preparing jatropha curcas shell-based activated carbon
A technology based on activated carbon and tung nut shell, applied in chemical instruments and methods, inorganic chemistry, non-metallic elements, etc., can solve the problems of long preparation time, environmental hazards, high energy consumption, etc., to improve yield, reduce pollution, improve effect of structure
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Embodiment 1
[0015] Put the prepared jatropha shell in a carbonization furnace, raise the temperature to 800°C at a heating rate of 20°C / min and keep it warm for 0.5 hours, and crush the obtained carbonized material to 4 to 20 meshes as an activated material. The temperature was raised to 600°C at a heating rate of ℃ / min, kept for 10 minutes, and then raised to 950°C at a heating rate of 15°C / min, and activated with a water vapor flow rate of 1.21g / min for 35 minutes to obtain a finished activated carbon product. The iodine adsorption value is 1165.3mg / g, and the yield is 29.2%.
Embodiment 2
[0017] Put the prepared jatropha shell in a carbonization furnace, raise the temperature to 800°C at a heating rate of 30°C / min and keep it warm for 1 hour, and crush the obtained carbonized material to 4 to 6 mesh as the activated material. Raise the temperature to 600°C at a heating rate of ℃ / min, keep it warm for 10 minutes, then raise the temperature to 870°C at a heating rate of 10°C / min, and activate with a water vapor flow rate of 4.3g / min for 50 minutes to obtain a finished activated carbon product. The iodine adsorption value is 1087.1 mg / g, and the yield is 23.7%.
Embodiment 3
[0019] Put the prepared jatropha shell in a carbonization furnace, raise the temperature to 800°C at a heating rate of 20°C / min and keep it warm for 0.5 hours, and crush the obtained carbonized material to 4 to 6 mesh as the activated material. Raise the temperature to 600°C at a heating rate of ℃ / min, keep it warm for 8 minutes, then raise the temperature to 960°C at a heating rate of 12°C / min, and activate with a CO2 flow rate of 100ml / min for 40 minutes to obtain a finished activated carbon product. The iodine adsorption value is 1143.1mg / g, and the yield is 31.3%.
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