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223 results about "Reagent standard" patented technology

Standards are used in analytical chemistry. Here, a primary standard is typically a reagent which can be weighed easily, and which is so pure that its weight is truly representative of the number of moles of substance contained.

Method for treating coking wastewater

The invention discloses a method for treating coking wastewater, which belongs to the field of wastewater treatment. The method comprises the following steps that: wastewater of a coking plant enters a regulating reservoir for the adjustment of water quality and water amount, and orderly enters a hydrolytic tank, an anaerobic tank, a preaeration tank, a preliminary sedimentation tank, an aerobic tank, a secondary sedimentation tank and a coagulation reaction tank for treatment, wherein the hydrolytic tank and the preaeration tank are filled with a bio-cord filler; the sludge of the preliminary sedimentation tank refluxes into the hydrolytic tank and the anaerobic tank respectively; a clarifying solution of the secondary sedimentation tank refluxes into the anaerobic tank; and the aerobic tank adopts a moving bed bio-film reactor. The bio-cord filler adopted in the invention has short film formation time and high biomass, does not need repeated washing, and has strong shock resistance; and the moving bed bio-film reactor can fix a large amount of nitrobacteria with long generation time, and has no the problem of blocking. The method can remove high-concentration ammonia nitrogen and organic substances in the coking wastewater, and the COD and the ammonia nitrogen of treated effluent can synchronously achieve the primary standard of the national integrated wastewater discharge standard (GB9878-1996).
Owner:NANJING UNIV

Manufacturing method and fixture of integral bladed-disk wax mold

The invention discloses a manufacturing method and a fixture of an integral bladed-disk wax mold. According to the invention, an integral bladed-disk wax pattern is divided into single blades and a disk shaft. Processes of separated pressing, precise fixture positioning and wax mold welding assembling are adopted. The integral wax pattern is precisely cast. According to the invention, the disk shaft is fixed on an assembling fixture; the blades are sequentially positioned on positioning points on the fixture, and are welded onto the disk shaft. Blade bodies and channel inner walls with high precisions are adopted in the positioning of the blades, such that good consistency is provided for the blades. When the wax pattern is assembled, positioning points are positioned on the blade bodies;blade body positioning points are consistent with processing positioning points, primary standards of cold and hot processing are consistent, such that blade dimensional precision of the whole cast is optimally improved, throat areas between blades are ensured, and flow rate homogeneity is ensured. Positioning parts of the fixture can be adjusted according to measured dimensions of parts, such that the volume of flow rate can be changed according to directional positions of angles of the blades. Therefore, repairing or even rejecting risks caused by unqualified integral mold dimensions are avoided, production period is saved, and production cost is reduced. With the method provided by the invention, hard processes are turned easy, product precision is improved, and production efficiency is improved.
Owner:AECC AVIATION POWER CO LTD

Process method for treating coking wastewater

The invention discloses a process method for treating coking wastewater. The process method solves the technical problems that a micro-electrolysis method has hardening, channeling and narrow applicability of a pH range and a biochemical treatment process has long flow, large occupied area, poor impact load resistance and high expense. The method comprises a physical-chemical treatment unit consisting of a micro-electrolysis reactor and a settling tank; in the micro-electrolysis reactor, scrap iron, scrap copper and a lightweight blocky material are used as fillers; the pH of inlet water is between 2.0 and 6.0; the waterpower retention time is between 20 and 60 minutes; the method adopts air aeration; the method also comprises a filtering type inner circulating three-phase fluidized bed reactor biochemical treatment unit, and immobilized activated sludge balls are utilized to realize simultaneous denitrification and decarburization; the pH of inlet water is between 7.2 and 8.5; the concentration of dissolved oxygen is between 2 and 6mg/L; the temperature is between 28 and 32 DEG C; the waterpower retention time is between 20 and 40h; the COD of outlet water reaches secondary standard of integrated wastewater discharge standard; and volatile phenol, ammonia nitrogen and chroma reach primary standard of integrated wastewater discharge standard.
Owner:NANJING UNIV OF SCI & TECH

Tower type earthworm and ecological filter for treating sewage

The invention provides a combined process of tower angleworm bio-filters and constructed wetlands for treating the domestic sewage. The combined process comprises the following steps: firstly, the sewage enters a hydrolysis-acidification pool and stabilizes after the action, and the water quantity is adjusted; secondly, the domestic sewage in the hydrolysis-acidification pool is distributed into a hydrolysis-acidification pool for removing COD, total nitrogen, nitrogen-nitrogen, total phosphorus and pathogeny microbes; and thirdly, the tail water in the second step enters a constructed wetland to be subjected to strengthening treatment, thereby building a suitable waterfront surroundings landscape, or the tail water is recycled by serving as reclaimed water. The combined process has the following advantages: firstly, the system hydraulic loading is high, and the surface hydraulic loading can reach 1m<3>/m<2>*d, thereby greatly saving land; and secondly, under the high hydraulic loading, the total nitrogen removal rate of the system can reach more than 85 percent; the removal rates of other materials in the system are all more than 90 percent, the effluent reaches the primary standard of the national sewage comprehensive emission standard (GB8978-1996), and reaches the miscellaneous domestic water quality standard of the PRC construction standard (CJ25.1-89), thereby being able to be recycled by serving as the reclaimed water.
Owner:NANJING UNIV

Device and method for processing restaurant wastewater

ActiveCN102145967AIncrease dissolved oxygenImprove the efficiency of degrading pollutantsMultistage water/sewage treatmentActivated sludgeElectrolysis
The invention discloses a device and a method for processing restaurant wastewater. A ferrallitic sheet is used as an anode and a graphite sheet is used as a cathode to carry out pulse direct current electrolysis on the restaurant wastewater so as to cause an electrocoagulation reaction; simultaneously ultrafine ozone bubbles are fed into an electrocoagulation reaction region to strengthen the electrocoagulation reaction, so that ferrous irons Fe2+ generated in the electrolysis process is rapidly converted into ferric irons Fe3+, the volume of flocculate becomes larger and the flocculate precipitates more efficiently to remove most of pollutants in the wastewater; sludge generated in the electrocoagulation process enters an activated sludge reactor and a sludge concentrating and extruding device; and clear water containing a little amount of organic matter enters an aeration-ozone-ultraviolet combined treatment degradation tank and a photocatalyst micro filtration membrane, and finally outflows through a fine porous sand filtering tank. The produced water can reach the primary standard in the industry. The processing method has high impact-load resistance. The outlet water quality is stable. In the engineering, consumables have long service life. Therefore, the processing cost of the restaurant wastewater can be greatly reduced.
Owner:TAIDEA TECH ZHONGSHAN

Treating method for phosphoric waste water and sludge generated in production process of phosphatic compound fertilizer

The invention discloses a treating method for phosphoric waste water and sludge generated in the production process of a phosphatic compound fertilizer, which comprises the following steps: adding lime milk into the phosphoric waste water to be treated firstly, and controlling a pH value to be 5-6; carrying out neutralization reaction for the first time; adding a PAM flocculating agent for flocculation reaction and then carrying out separation of mud and water; adding the lime milk in the aqueous phase again, and controlling the pH value to be 10-11 for the neutralization reaction for the second time; and adding the PAM flocculating agent again for the flocculation reaction and then carrying out the separation of mud and water, wherein the aqueous phase reaches a effluent standard after filtration. The invention realizes the multiplexing or the standard-reaching discharge of the waste water, the zero release of the sludge, accords to the developing direction of the energy saving and emission reduction and circular economy. The clear liquid treated by the process of the invention contains 0.4-0.5mg/L of phosphate (calculated by being based on P2O5), 8-9mg/L of F and 60-80mg/L of COD, meets the primary standard emission requirement of GB8978-1996, the ultimate clear liquid can be returned to a phosphoric acid device for multiplexing, and also be directly discharged after reaching standards; and the sludge produced by the filtration comprises the following main components: calcium phosphate, calcium fluoride, calcium carbonate and calcium sulfate, which can be totally reused as phosphorite resources.
Owner:中化重庆涪陵化工有限公司

Rural domestic sewage treatment process

The invention discloses a rural domestic sewage treatment process. In the rural domestic sewage treatment process, a fine grid is used in a pretreatment process to remove large particle pollutants in sewage; an underground anaerobic digester is adopted to carry out hydrolysis acidification treatment so as to provide good conditions for a subsequent aerobic process; a micro power aerobic filter bed organically combines a solar energy micro power technology with an aerobic filter bed technology; a system is supplied with aeration power by solar energy; and a grading packing layer is arranged in the filter bed so as to realize low consumption and high efficiency treatment of the sewage. The rural domestic sewage treatment process particularly comprises the following procedures that after passing through the fine grid, the sewage enters the anaerobic digester; an elastic packing or a flexible packing is arranged in the anaerobic digester; and yielding water flowing out from the anaerobic digester enters the micro power aerobic filter bed system to be treated, wherein CODcr (Chemical Oxygen Demand), NH3-N (index of the ammonia nitrogen content in the sewage) and TP (total phosphorus) of the yielding water can reach the primary standard B of Discharge Standard of Pollutants for Municipal Wastewater Treatment Plant (GB18918-2002). Due to the adoption of the rural domestic sewage treatment process, the treatment efficiency and the treatment degree of the domestic sewage can be improved. The rural domestic sewage treatment process is not limited by areas or air temperature and has small occupied area and low operation cost.
Owner:ENVIRONMENTAL SCI RES & DESIGN INST OF ZHEJIANG PROVINCE

Zero grain consuming full liquid state method for producing vinegar with solid state fermentation flavor

The invention discloses a production method of table vinegar with zero grain consumption and complete liquid state and solid fermentation flavor. The method comprises a material blending process, an acetic fermentation process, a post maturation flocculation process, a refining sterilization process, and a mixing process, wherein, the material blending process adopts the steps that at least two of solid state liquor making concomitant flavoring liquid, grain stillage squeezed fluid, ending liquor, and ending water are blended, and the total acid content of acetometer in the mixed liquor is 0.48 to 6.5 g/100 ml, and the alcohol content is 0 to 6.5 V/V percent; the acetic fermentation process adopts the steps that that the mixed liquor is accessed into acetic acid bacteria liquor, the weight of the mixed liquor is 10 percent of the weight of the acetic acid bacteria, and the mixed liquor is ventilated to be fermented at 32 to 36 DEG C, and the fermentation is finished when the total acid content of acetometer reaches 5.5 to 6.5 g/100 ml; the post maturation flocculation process adopts the steps that that the fermentation liquor is accessed into aged bentonite abstracted filter liquor, and the weight of the fermentation liquor is 0.7 to 0.8 percent of the weight of the bentonite; then the vinegar is prepared according to the regular refining sterilization process and the mixing process. The invention has the advantages that the process period is short, the cost is low, the grain consumption is zero, the vinegar tastes good, the nutritive value is high, and the vinegar meets the the primary standard of the national value fermentation GB2719-2003. The effective constituents in the flavoring liquid, the grain stillage squeezed fluid, the ending liquor and the ending water can be fully used, the vinegar can effectively protect the environment from pollution, and the invention can be popularized in liquor manufacturing enterprises.
Owner:SICHUAN TUOPAI SHEDE WINE

Method for treating wastewater of fibre-board plant

The invention discloses a method for treating wastewater of a fibre-board plant. The method is characterized by including the combination of technical skills of the following three parts: a pretreatment system, a biochemical treatment system and an aftertreatment system; wastewater from production is respectively led into a filter and a centrifuger; after being processed by the step of slag removal, the wastewater flows into a horizontal sedimentation tank, a pre-aeration regulation tank and an iron aeration tank or a vertical sedimentation tank and then is processed by dissolved air flotation; the discharged water is respectively pumped into a turn-back flow anaerobic tank with filter materials and an oxidation tank and then flows into an inclined-tube sedimentation tank to settle; and after suspended substances in the wastewater are removed by a filtration tank, the wastewater is discharged while reaching standards. The method has the advantages that the efficiency of removing the suspended substances is high, water is circularly and repeatedly used, water consumption is reduced, the discharge amount of the wastewater can be reduced by more than 300 tons each day, the occupation of land of equipment is low, the operation is simple, and the running cost is low. Extruded wood slag and sludge can be used as energy to be led into an energy centre to combust, secondary pollution is not caused, and the treated wastewater can meet the requirement of primary standard in the Integrated Wastewater Discharge Standard GB8978-1996.
Owner:GUANGXI FENGLIN WOOD IND GRP CO LTD

Method for enhancing petroleum pollution removing effect of seawater

The invention belongs to the technical field of environmental pollution, in particular to a method for enhancing the petroleum pollution removing effect of seawater. The method comprises the following steps of: culturing high-yield biological surfactant bacteria and efficient petroleum degrading bacteria cultured and screened in a biological trickling filter in a mixed way by taking chitosan as a carrier, and performing freeze drying to obtain a microbial agent (bacterial powder); and treating petroleum pollution simulation seawater with the bacterial powder, wherein three days later, the initial concentration is 1,700 mg/L, the salinity is 3 percent, the removing rate of total petroleum hydrocarbon in the simulation seawater is over 95 percent, and the total petroleum hydrocarbon concentration in the seawater is lower than the primary standard in the Effluent Standards for Oil-Bearing Waste Water from Offshore Petroleum Development Industry. In the method, chitosan is taken as a carrier, so that microorganisms better float on the sea level and are tightly contacted with pollutants on the surface of seawater, and the petroleum removing rate is increased; moreover, the treatment cost of oil stains is reduced greatly; and the production process of the bacterial powder is safe, the application method is simple, and secondary environmental pollution is prevented.
Owner:FUDAN UNIV

Method for processing waste water/gas from tungsten smelting and a device thereof

The invention relates to a method for processing waste water / gas from tungsten smelting and a device thereof. The method is to directly implement the processing of the waste water / gas by utilizing alkali waste water, which is generated by extracting ammonium tungstate from tungsten ores by an ion exchange method, and by utilizing smoke gas generated by a boiler furnace, and the method comprises the following steps of: cyclone dust removal, spray dust removal, desulfurization, deamination, controlling the temperature of the primarily dust-removed smoke gas of the boiler furnace in a range from 140-200 DEG C, diffusing from bottom to top the air quantity of 13000-18000 m<3> / H and controlling the flow quantity from top to bottom in a range from 13-15 m<3>H, spraying the alkali waste water for exchange absorption for removing fine particle dusts and SO2 in the smoke gas and free ammonia in the alkali waste water, exhausting net gas after the spraying absorption to the air and discharging purified water after deposition; the device for realizing the method for processing waste water / gas from tungsten smelting comprises; a water pump, a multitubular cyclone dust extractor, a dust-removing desulfurization deamination nitrogen column and a water processing pond. The invention has the advantages of simple technological steps, small investment of the device, easy operation, low processing cost and primary standard exhaust of the waste water / gas.
Owner:FUJIAN JINXIN TUNGSTEN

Treating technology for chemical RO concentrated water

The invention relates to a treating technology for reverse osmosis (RO) concentrated water after water reuse in a chemical membrane method. The technology comprises the steps that firstly, matter such as lime or sodium hydroxide which is alkaline in an aqueous solution is put in RO concentrated water effluent to enable the pH of the concentrated water to be about 10-11.5; secondly, flocculent precipitation is performed in a mechanical accelerating clarification tank to reduce the hardness of the wastewater and remove heavy metal and reducing metal ions; thirdly, the effluent directly enters an ozone reaction tank after the RO concentrated water passes through the mechanical accelerating clarification tank, and then ozone tank effluent enters a biological activated carbon filter bed device to further remove pollutants and turbidity in the RO concentrated water, so that the wastewater effluent can meet the national primary standard (the CODcr is smaller than or equal to 60 mg/L). According to the treating technology, further treatment is performed on the concentrated water generated after the water is reused through the front stage of biochemistry, ultrafiltration and reverse osmosis for the production wastewater in chemical industry to achieve the purpose of direct discharge, therefore, the pollution treatment ability of enterprises can be improved, the total pollutant discharge amount is reduced, and the effects of energy conservation and emission reduction, clean production and sustainable development are achieved.
Owner:博瑞德环境集团股份有限公司

Clean production method of rubber vulcanizing accelerator TBBS

The invention discloses a clean production method of a rubber vulcanizing accelerator TBBS, relating to the clean production method of the rubber vulcanizing accelerator TBBS. The cleaning production method is characterized by comprising the following steps of: a, preparing mixing liquid by 1 wt% of accelerators M, 1.5 to 2.4 wt% of tert-butylamine, 0.01 to 0.02 wt% of catalysts and 8 to 14 wt% of water; b, dropwise adding 27.5 wt% hydrogen peroxide in the solution with the flow rate of 50 to 110 ml / min, wherein the oxidizing temperature is 30 to 50 DEG C, and the oxidizing time is 120 to 180 min; c, sampling, detecting by using ammonium sulfate and starch potassium iodide reagents, and stopping adding the hydrogen peroxide when materials are brown in color through detection; and d, filtering and drying to obtain the rubber vulcanizing accelerator TBBS. The invention has the advantages of simple production process, low raw material consumption, high yield, cleanness, environment protection and energy saving; the yield of the accelerator TBBS is higher than 99%, and the product quality is higher than the national primary standard; waste water generated in the technology contains no salt and is easy for biochemical treatment; and the invention reduces environmental pollution and equipment corrosion.
Owner:河南省开仑化工有限责任公司

Bonding agent of baking-free bricks prepared from drilling well solid waste materials

The invention relates to a bonding agent of baking-free bricks prepared from drilling well solid waste materials, which is applied to the field of treating petroleum drilling well solid waste materials into resources for preparing baking-free bricks. The bonding agent comprises the following ingredients in parts by weight: 3.3 to 8 of polyaluminium chloride, 6 to 25 of phosphogypsum, 10 to 26 of lime, 20 to 60 of fly ash and 4.4 to 12 of ferrous sulfate. A method for using drilling well solid waste materials for preparing the baking-free bricks comprises the following steps that: the baking-free bricks are prepared from the following ingredients in parts by weights: 10 to 22 of bonding agents of baking-free bricks prepared from drilling well solid waste materials, 30 to 55 of drilling well solid waste materials and 35 to 45 of crude aggregate; and the ingredients are uniformly mixed, are extruded and formed through a baking-free brick machine, and are maintained for 14 to 21 days to prepare the baking-free bricks. The invention has the advantages that the baking-free bricks can be prepared, and through the analysis via the sampling and the water soaking experiments on the baking-free bricks, all contaminant indexes reach the primary standard. Through the examination according to the standard JC422-1991, the detected items of the samples reach the requirements of the standard.
Owner:PETROCHINA CO LTD

High-intensity magnesite cement board and preparation method thereof

The invention relates to a high-intensity magnesite cement board and a preparation method thereof. The constituent raw materials are rice hull, an additive, magnesite powder, magnesium chloride modified water, phosphoric acid, a defoaming agent and glass fiber cloth. The preparation method comprises the following steps of: (1) starting a machine and stirring the rice hull and the additive for 5 minutes according to a weight ratio, adding the magnesium chloride modified water, adding the magnesite powder while stirring, after 10 minutes, adding the phosphoric acid and the defoaming agent, and after 5 minutes, forming mixed slurry; (2) adding a layer of the glass fiber cloth in the mould, injecting the mixed slurry on the glass fiber cloth, and vibrating a rolling plate; (3) placing the mould on a steel frame and feeding to a curing chamber; and (4) after leaving the frame and demolding, and opening a mortise and tenon joint of a mortise by utilizing a machine so as to obtain a finished product. The high-intensity magnesite cement board, provided by the invention, has the advantages of scientific composition and artful compatibility of raw materials, good compaction, high intensity and good water tolerance of the formed board, stable neutralization of oxygen ions, and safety use, after detection and identification of a national authority compartment, all indexes reach primary standard of nation, and the high-intensity magnesite cement board is suitable for high-speed rail construction, flyovers, stadiums, airport baffles of a waiting room, an inner wallboard, an outer wallboard and a floor substrate.
Owner:TIANJIN TIANYI DINGSHENG PANEL CO LTD
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