Corrosion inhibitor for oil-gas field equipment corrosion resistance and preparation method thereof
A corrosion inhibitor, oil and gas field technology, applied in the corrosion inhibitor and its preparation, in the field of petroleum industry anticorrosion, to achieve the effects of improved polarization resistance, low cost and high corrosion inhibition rate
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example 4
[0037] Example 4 is the evaluation of the corrosion inhibition performance of the corrosion inhibitor by electrochemical method. The three-electrode system of A3 steel sample-platinum electrode-saturated potassium chloride electric shock was used to measure its electrochemical behavior in saturated hydrogen sulfide aqueous solution with and without the addition of corrosion inhibitor. The purity of industrial-grade pyridine is 50% to 60%, and it is rectified. Its main components are pyridine, pyridine, and quinoline derivatives.
example 1
[0039] Add distilled water to ferric sulfate until it is completely dissolved, then slowly add n-butylamine dropwise therein until a uniform and stable solution is formed, the mass ratio of ferric sulfate to n-butylammonium is 1:1; industrial grade pyridine (purity about 55 %) is placed in a rectifying device, the temperature is adjusted to 250 degrees Celsius, and the pyridine fraction is collected for subsequent use. N-butylammonium salt, pyridine, sodium molybdate and 95% ethanol are formulated as corrosion inhibitor according to 40%: 10%: 5%: 45%.
[0040] The test was carried out in a test tube filled with H 2 S saturated aqueous solution 10mL, put a 10×10×3 steel sheet sample prepared with A3 steel in each test tube, a total of 10, 5 of which add corrosion inhibitor (6-10 drops each), 5 as a blank sample. After the test tube is sealed, it is placed in a constant temperature water bath device at 50°C, and the test is carried out in a static state for 5 days. After takin...
example 2
[0042] Add distilled water to ferric sulfate until it is completely dissolved, then slowly add n-butylamine dropwise therein until a uniform and stable solution is formed, the mass ratio of ferric sulfate to n-butylammonium is 1:1; industrial grade pyridine (purity about 55 %) is placed in a rectifying device, the temperature is adjusted to 250 degrees Celsius, and the pyridine fraction is collected for subsequent use. n-Butyl ammonium salt, pyridine, sodium molybdate and 95% ethanol are formulated as corrosion inhibitor according to 30%: 20%: 5%: 45%.
[0043] The test was carried out in a 1L jar with 400mL of H2S aqueous solution inside, and a 10×10×3 steel sheet sample made of A3 steel was hung on the bracket so that it was above the liquid level in the bottle. There are two bottles in total, each with 5 tablets, one of which is added with corrosion inhibitor (corrosion inhibitor is placed in a small beaker, about 3ml, and then placed in a jar), and one is blank. Put the s...
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