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Method for producing lube base oil

A lubricating oil base oil and production method technology, which is applied in the petroleum industry, hydrocarbon oil treatment, hydrotreating process, etc., can solve the problems of low yield of lubricating oil base oil, and achieve high yield and clear and transparent appearance

Active Publication Date: 2010-06-30
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The object of the present invention is to overcome the low yield of lubricating oil base oil existing in the above-mentioned prior art, and provide a kind of production method of lubricating oil base oil with higher yield

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The raw material adopts the mixed oil of Fischer-Tropsch synthetic wax and hydrocracking tail oil with a weight ratio of 1:1. The properties of Fischer-Tropsch synthetic wax are shown in Table 1, and the properties of hydrocracking tail oil are shown in Table 2. The properties of mixed oil See Table 3.

[0029] Table 1

[0030] project

F-T synthetic wax

Freezing point (℃)

92 (melting point)

Sulfur content (μg / g)

<5

Nitrogen content (μg / g)

13

Oxygen content (μg / g)

5000

Distillation range (℃)

initial boiling point

10%

30%

50%

70%

90%

95%

D-1160

128

384

455

492

529

582

618

[0031] Table 2

[0032] project

Hydrocracking tail oil

Kinematic viscosity (mm 2 / s), 100℃

4.958

Freezing point (℃)

39

Saturated hydrocarbon (weight%)

99.4

Aromatics (weight%)

0.6

S content (μg / g)

...

Embodiment 2

[0043] Lubricant base oil products are produced in the manner described in Example 1, the difference is that the weight ratio of Fischer-Tropsch synthetic wax to hydrocracking tail oil in the raw material is 0.2, the properties of the mixed oil are shown in Table 5, and first add The conditions of hydrofinishing reaction, hydroisomerization reaction and post-hydrofinishing reaction are different and are shown in Table 6.

[0044] The properties of the product obtained and the yield of the product are shown in Table 10.

[0045] table 5

[0046] project

mixed oil

Kinematic viscosity (mm 2 / s), 100℃

4.755

Freezing point (℃)

75

S content (μg / g)

<5

N content (μg / g)

<5

[0047] Table 6

[0048] Process conditions

Embodiment 3

[0050] Lubricant base oil products are produced in the manner described in Example 1, the difference is that the weight ratio of Fischer-Tropsch synthetic wax to hydrocracking tail oil in the raw material is 5, and the properties of the mixed oil are shown in Table 7, and firstly add The conditions of hydrofinishing reaction, hydroisomerization reaction and post-hydrofinishing reaction are different and are shown in Table 8.

[0051] The properties of the product obtained and the yield of the product are shown in Table 10.

[0052] Table 7

[0053] project

mixed oil

Kinematic viscosity (mm 2 / s), 100℃

3.056

Freezing point (℃)

87

[0054] project

mixed oil

S content (μg / g)

<5

N content (μg / g)

<5

[0055] Table 8

[0056] Process conditions

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Abstract

The invention provides a method for producing a lube base oil. The method comprises the steps of: making raw materials and the hydrogen gas contact a hydroisomerization catalyst under hydroisomerization reaction conditions to perform the hydroisomerization reaction; making the product of the hydroisomerization reaction contact a hydrorefining catalyst under hydrorefining reaction conditions to perform the hydrorefining reaction; and fractionating the product of the hydrorefining reaction, wherein the raw material is the mixed oil of a Fischer-Tropschb synthetic wax and a hydrocracking tail oil. The quality of the lube base oil product obtained by adopting the method of the invention is high, the yield is relatively high, and the obtained product is clear and transparent without being processed by a defogging step; and meanwhile, the process is very simple and the operation control is easy.

Description

technical field [0001] The invention relates to a production method of lubricating oil base oil. Background technique [0002] The lubricating base oil produced by hydrogenation has the advantages of good quality, high yield, and large operating flexibility, especially the production of low-viscosity base oil for the deployment of long-span lubricating oil, that is, low dynamic viscosity (CCS) and low volatility Type III oils with high degrees can only be produced by hydrogenation. Therefore, hydrogenation production technology is developing rapidly abroad. Major oil companies have developed their own hydrogenation process and realized industrial application. The catalytic dewaxing technology, which was widely used in industry in the last century, is being replaced by a new and more superior isomerization dewaxing technology, except for its superiority in the application of raw materials containing less wax due to the technology itself. [0003] Representative isomerizati...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G65/04
Inventor 王鲁强郭庆洲王轶凡黄卫国夏国富
Owner CHINA PETROLEUM & CHEM CORP