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Silicon steel hearth roll sleeve and preparation method thereof

A hearth roller and silicon steel technology is applied in the field of carbonaceous raw materials to prepare high temperature metallurgical materials, which can solve the problems of long cycle, high energy consumption, complex production process, etc., and achieves low porosity, high bulk density, and improved oxidation resistance. performance effect

Inactive Publication Date: 2012-09-19
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the special properties of silicon steel sheets, there are very unique performance requirements for hearth roll sleeves. Therefore, the production process of hearth roll sleeves is very complicated, not only long in cycle but also high in energy consumption.
As described in patents JP57137419A, JP57140377A, 1092324A, CN1117479, CN1994967, and CN2199206, the silicon steel hearth roller sleeve and its preparation and surface treatment methods all go through batching, compression molding, roasting, vacuum infiltration, ultra-high temperature firing, and mechanical processing. Silicon steel hearth roller sleeves are prepared by other processes, the production process is complicated, the cycle is long, and the energy consumption is high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] A silicon steel hearth roll casing and a preparation method thereof. Mix 2-6wt% large particles of dense carbonaceous raw materials, 2-6wt% small particles of dense carbonaceous raw materials, 90-95wt% fine powder of dense carbonaceous raw materials and 0.3-0.8wt% Si micropowder, and add the above-mentioned 5-8wt% phenolic resin, mixed and milled for 20-30 minutes.

[0014] The mixed material after mixing and milling is pressed into silicon steel hearth roller sleeve tube billet, kept at 180-200°C for 6-8 hours, then placed in a sealed pressure vessel, and kept under the condition of vacuum degree of 10000-15000Pa 20-30 minutes, then open the valve and inject liquid phenolic resin until the tube blank is completely soaked, pump air to a vacuum degree of 10000-15000Pa, and keep it for 20-30 minutes; finally, keep it warm for 8-10 minutes at a high temperature of 2100-2150℃. Hours, using lathes and grinders to process the high-temperature fired silicon steel hearth rolle...

Embodiment 2

[0016] A silicon steel hearth roll casing and a preparation method thereof. Mix 6-10wt% large particles of dense carbonaceous raw materials, 2-6wt% small particles of dense carbonaceous raw materials, 85-90wt% fine powder of dense carbonaceous raw materials and 0.8-1.2wt% Si micropowder, and add the above-mentioned 6-10wt% phenolic resin, mixed and milled for 20-30 minutes, and pressed into silicon steel hearth roller sleeve tube billet.

[0017] The mixed material after mixing and milling is pressed into silicon steel hearth roller sleeve tube billet, kept at 180-200°C for 6-8 hours, then placed in a sealed pressure vessel, and kept under the condition of vacuum degree of 10000-15000Pa 20-30 minutes, then open the valve and inject liquid phenolic resin until the tube blank is completely soaked, pump air to a vacuum degree of 10000-15000Pa, and keep it for 20-30 minutes; finally, keep it warm for 8-10 minutes at a high temperature of 2050-2100°C Hours, using a lathe and a gri...

Embodiment 3

[0019] A silicon steel hearth roll casing and a preparation method thereof. Mix 2-6wt% large particles of dense carbonaceous raw materials, 6-10wt% small particles of dense carbonaceous raw materials, 85-90wt% fine powders of dense carbonaceous raw materials and 1.2-1.6wt% Si micropowder, and add the above compounding 8-12wt% phenolic resin is mixed and milled for 20-30 minutes, and then pressed into a silicon steel hearth roller sleeve tube billet.

[0020] The mixed material after mixing and milling is pressed into silicon steel hearth roller sleeve tube billet, kept at 200-220°C for 4-6 hours, then placed in a sealed pressure vessel, and kept under the condition of vacuum degree of 15000-20000Pa 15-25 minutes, then open the valve and inject liquid phenolic resin until the tube blank is completely soaked, evacuate to a vacuum degree of 15000-20000Pa, keep for 15-25 minutes; finally keep warm for 10-12 Hours, using a lathe and a grinder to process the high-temperature fired ...

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PUM

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Abstract

The invention relates to a silicon steel hearth roll sleeve and a preparation method thereof. The technical scheme of the method comprises the following steps of: mixing 2 to 10 weight percent of large particles of a dense carbon raw material, 2 to 10 weight percent of small particles of the dense carbon raw material, 80 to 95 weight percent of fine powder of the dense carbon raw material, and 0.3 to 2.0 weight percent of Si micro-powder, as well as 5 to 15 weight percent of phenolic resin based on the total amount of the raw materials; pressing the mixture into a blank of the silicon steel hearth roll sleeve after mixing and rolling, preserving the heat for 4 to 8 hours at the temperature of between 180 and 220 DEG C, placing the blank in a pressure vessel, maintaining the state for 15 to 30 minutes at the vacuum degree of between 10,000 and 20,000Pa, injecting liquid-state phenolic resin into the pressure vessel, pumping air until the vacuum degree is between 10,000 and 20,000Pa, and maintaining the state for 15 to 30 minutes; and finally, preserving the heat for 8 to 12 hours at the high temperature of between 1,950 and 2,150 DEG C, and machining the blank until the surface roughness is less than or equal to 12.5. The method has the advantages of simple process and low energy consumption; and the prepared product has the characteristics of high oxidation resistance, high strength, high abrasion resistance, low porosity, no nodule and capability of improving the quality of the silicon steel plate.

Description

technical field [0001] The invention belongs to the technical field of preparing high-temperature-resistant metallurgical materials from carbonaceous raw materials. In particular, it relates to a silicon steel hearth roller casing and a preparation method thereof. Background technique [0002] Since the 1980s, the iron and steel industry has developed a continuous annealing system to produce high-quality steel plates, and the carbonaceous hearth roll sleeves used in the continuous annealing furnace for the production of silicon steel plates play a key role. Due to the special properties of silicon steel sheets, there are very unique performance requirements for hearth roll sleeves. Therefore, the production process of hearth roll sleeves is very complicated, with long cycle times and high energy consumption. As described in patents JP57137419A, JP57140377A, 1092324A, CN1117479, CN1994967, and CN2199206, the silicon steel hearth roller sleeve and its preparation and surface ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66
Inventor 祝洪喜邓承继白晨刘奎然钟庆
Owner WUHAN UNIV OF SCI & TECH