Methods for making electronic devices
A technology for electronic devices and electrodes, which is applied in the field of electronic devices and the preparation of such electronic devices, and can solve problems such as electronic component failure and performance degradation
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preparation example 1
[0157] Surface-modified inorganic nanoparticles were formed by reacting silane with silica nanoparticles having an average particle size of 21 nanometers (nm). More specifically, 300 grams of Nalco 2327 colloidal silica available from Nalco Chemical Company (Naperville, Illinois) was placed in a bottle with a stir bar. 28 grams of a 25% by weight aqueous solution of carboxyethylsilanetriol sodium salt, obtained from Gelest, Inc., Morrisville, Pennsylvania, were added to the colloidal silica over a period of 10 minutes with stirring. A small amount of precipitate formed after addition of carboxyethylsilanetriol sodium salt, but the precipitate dissolved with additional stirring. The clear dispersion was then placed in an oven at 95°C for 20 hours. The percent solids of the surface-modified colloidal silica in water was measured to be 40% by weight based on weight loss after drying. The dispersion before drying was used in subsequent examples.
preparation example 2
[0159] A mixture containing 1.0 grams of starch (ICB 3000) from Tate & Lyle Public Company Limited (Decatur, Illinois), 12 grams of deionized water, 0.56 grams of 30% by weight aqueous A mixture of the ammonium hydroxide solution and 4.0 grams of the surface-modified colloidal silica dispersion of Preparation Example 1 was added to the vessel while mechanically stirring. After the starch was dissolved in the mixture, 2.0 g of (4-dimethylamino-1-[4,6-bis(4-carboxyphenylamino)-1,3,5-triazine-2- A chromophoric material represented by base] pyridinium chloride) is slowly added to the mixture while stirring. After the chromonic material was dissolved, 0.44 grams of a 10% by weight aqueous solution of an alkyl polyglucoside surfactant (Glucopon 425N) obtained from Cognis, Cincinnati, Ohio, was added to the mixture with stirring. Disposable syringe filters equipped with 5.0 microns (25 mm in diameter, which have a Versapore membrane that is a hydrophilic acrylic copolymer on a nonwo...
preparation example 3
[0169] A second bimetallic nanowire-containing PET film was prepared using the procedure of Preparation Example 2 with the same material concentration, except that the resulting mixture was based on a total amount of 30 g. The electrical surface conductivity of the resulting film was determined to be 22.1 millisiemens / square.
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