Processes for photolithography
A composition and photoresist technology, applied in the direction of photoengraving process of pattern surface, photoengraving process coating equipment, photosensitive material for opto-mechanical equipment, etc.
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Embodiment 1
[0070] Particles (including organic particles) used as substantially immiscible materials include Si-containing and fluorinated materials having carboxyl groups. These particles are commercially available, or can be easily synthesized, for example, by reacting one or more monomers with a crosslinker and an initiator compound (if necessary). The reactive monomer may have substituents such as fluorine, Si substituents, photoacid labile groups such as photoacid labile esters or acetals, and other basic soluble groups such as alcohols as needed. In Example 1 below, such particles were exemplarily synthesized using a variety of different monomers, and one of the monomers provided a photoacid labile group to the resulting polymer particles.
[0071] The substantially immiscible materials are present in the photoresist composition in relatively small amounts, but are still effective. For example, based on the total weight of the liquid photoresist composition, one or more substantially...
Embodiment 2
[0116] Example 2: Preparation of other carboxylic acid resins
[0117] The following carboxylic acid resin was prepared by the similar procedure of Example 1:
[0118] weight ratio
Embodiment 3
[0119] Example 3: Preparation of heterosubstituted carbocyclic aryl resin
[0120] The preparation of the hydroxynaphthalene terpolymer resin having the following structure is disclosed below:
[0121] x / y / z=65 / 10 / 25
[0122] 1. Reactor: Add 20 g of propylene glycol methyl ether acetate (PGMEA) into a 100 ml flask equipped with a magnetic stir bar, and place the flask in a 85°C hot bath while stirring and refluxing for condensation. Purge the reactor with dry nitrogen.
[0123] 2. Monomer / initiator solution: weigh 6.5g of 4,4,4-trifluoro-3-hydroxy-1-methyl-3-(trifluoromethyl)butyl-2-methacrylate, Add 1.0 g of hydroxyvinyl naphthalene, and 2.5 g of 2,3,3-trimethacrylate to a suitable container. Then 10.0 g PGMEA was added to the container. Shake the container to dissolve all the monomers, then place it in an ice bath to cool the monomer solution to 0°C. Then add 0.3 g of tert-butyl peroxyneodecanoate (triganox 23 initiator from Noury Chemicals) to the monomer container bottle, a...
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