Method for preparing cooked pepper resin
A technology of prickly ash resin and prickly ash, applied in the field of preparation of cooked prickly ash resin, can solve the problems of affecting product yield and quality, residual organic solvent and high operating temperature, and achieve the effects of high utilization rate, uniform extraction and high yield
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Embodiment 1
[0016] Zanthoxylum bungeanum was dried at 100°C for 60 minutes, with a moisture content of 10%, crushed into 60-mesh powder, and then filled into the extraction tank of a supercritical carbon dioxide extraction system with a filling factor of 85%, a temperature of 30°C, and a pressure of 35Mpa. Carbon dioxide enters the extraction tank from the bottom. After 2 hours of extraction, the Zanthoxylum bungeanum resin is separated into an open plastic tank in a separation tank with a temperature of 45° C. and a pressure of 15 MPa. The obtained Zanthoxylum bungeanum oleoresin is light yellow.
Embodiment 2
[0018] Green Zanthoxylum bungeanum was dried at 120°C for 40min, with a water content of 8.5%. After being crushed into 80-mesh powder, it was then filled into the extraction tank of a supercritical carbon dioxide extraction system with a filling factor of 90%, a temperature of 40°C, and a pressure of 40Mpa. Critical carbon dioxide enters the extraction tank from the bottom. After 1.5 hours of extraction, the Zanthoxylum bungeanum resin was separated into an open plastic tank in a separation tank with a temperature of 40° C. and a pressure of 10 MPa. The obtained Zanthoxylum bungeanum oleoresin is light yellow.
Embodiment 3
[0020] Dahongpao Zanthoxylum bungeanum was dried at 125°C for 45 minutes, with a moisture content of 8%, crushed into 60-mesh powder, and then filled into the extraction tank of a supercritical carbon dioxide extraction system with a filling factor of 90%, a temperature of 35°C, and a pressure of 30Mpa. Supercritical carbon dioxide enters the extraction tank from the bottom. After 2.5 hours of extraction, the Zanthoxylum bungeanum resin is separated into an open plastic tank in a separation tank with a temperature of 50° C. and a pressure of 20 MPa. The obtained Zanthoxylum bungeanum oleoresin is light yellow.
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