Cold-resistant acrylate rubber as well as preparation and application thereof

A technology of acrylate and methyl acrylate, which is applied in the field of synthetic acrylate rubber, which can solve the problems of easy roll sticking, poor strength, oil resistance, poor overall performance, and poor post-processing performance, and achieve high strength and post-processing performance. Good effect with good physical and mechanical properties

Inactive Publication Date: 2011-03-30
袁文阳
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The cold-resistant acrylic rubber used in the domestic automobile industry has been occupied by foreign rubber for a long time. The minimum operating temperature of domestic acrylic rubber cannot reach -30°C, or although it can meet the cold-resistant requirements, its comprehensive properties such as strength and oil resistance are not good. Roller sticking is prone to occur during post-processing, resulting in poor post-processing performance

Method used

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  • Cold-resistant acrylate rubber as well as preparation and application thereof
  • Cold-resistant acrylate rubber as well as preparation and application thereof
  • Cold-resistant acrylate rubber as well as preparation and application thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0033] Rubber was prepared according to the formula and process parameters in Table 1.

[0034] preparation steps

[0035] 1) Basic monomer ingredients: mix methyl acrylate, ethyl acrylate, butyl acrylate, ethyl methoxyacrylate, and vulcanization point monomers in a premixing tank in proportion to make a hydrocarbon phase solution for later use;

[0036] 2) Put the emulsifier into the reaction kettle, fully stir for standby;

[0037] 3) Emulsion polymerization: Put the hydrocarbon phase solution prepared in step 1) into the reaction kettle in proportion, stir well, add an initiator in proportion between 5-50°C to initiate the reaction, control its reaction speed and peak value, until the hydrocarbon phase reaction is complete;

[0038] 4) Salt polymerization: Send the fully reacted glue in step 3) to the coagulation pool with compressed air to mix with the coagulant, break the emulsion at a temperature of 20-70°C, and coagulate into a white solid elastomer, which is ready af...

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Abstract

The invention discloses a cold-resistant acrylate rubber as well as preparation and application thereof. As the total weight of acrylate monomer and vulcanization point monomer is 100%, the cold-resistant acrylate rubber comprises the following raw materials in percentage by weight: 0-30% of methyl acrylate, 20-50% of ethyl acrylate, 30-60% of butyl acrylate, 8-30% of methoxyl ethyl acrylate, 1-5% of vulcanization point monomer, 0.0001-1% of initiator, 1-10% of emulsifying agent and 2-40% of flocculant. The cold-resistant acrylate rubber is prepared by using an emulsion polymerization method, and can be used for automobiles, motorcycles, transformers, rubber tubes and the like.

Description

technical field [0001] The invention is a synthetic acrylic rubber, in particular to cold-resistant acrylic rubber and its preparation and application. Background technique [0002] Domestic cold-resistant acrylic rubber is an elastomer formed by emulsion polymerization with ethyl acrylate as the main monomer and vinyl monochloroacetate as the vulcanization point monomer. Because its main chain is a saturated structure, it is oil-resistant and resistant. properties such as oxidation. For the cold-resistant type, the minimum operating temperature of domestic acrylic rubber is about -23°C, which cannot meet the requirements of auto parts for acrylic rubber. [0003] The cold-resistant acrylic rubber used in the domestic automobile industry has been occupied by foreign rubber for a long time. The minimum operating temperature of domestic acrylic rubber cannot reach -30°C, or although it can meet the cold-resistant requirements, its comprehensive properties such as strength and...

Claims

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Application Information

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IPC IPC(8): C08F220/18C08F220/14C08F220/28C08F218/08C08F2/24
Inventor 袁文阳
Owner 袁文阳
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