Resistance switch material in Ag/Ag2S core/shell nanometer structure and preparation method thereof
A resistance switch and nanostructure technology, applied in the coating and other directions, can solve the problems of weak electronic signal of resistance switch, difficult to achieve industrial amplification, difficult application, etc., to achieve the effect of easy mass production, convenient industrial amplification, and enhanced current signal
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[0036] Example 1
[0037] In 50 ml of ethylene glycol, add 10 g of PVP (K30), magnetically stir, heat to 190°C, then add 0.1 g of silver nitrate, keep at 190°C for 5 minutes; then, add 5 mg of sulfur powder to react at 190°C After 10 minutes, the precipitate obtained from the reaction was washed with ethanol and dried at 40~80℃ to obtain Ag / Ag with a particle size of 10~15 nm 2 S core / shell nanocrystals.
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[0038] Example 2
[0039] In 50 ml of ethylene glycol, add 10 g of PVP (K30), magnetically stir, heat to 180 ℃, then add 0.5 g of silver nitrate, keep at 180 ℃ for 10 minutes; then, add 20 mg of sulfur powder, at 180 ℃ After reacting for 10 minutes, the precipitate obtained from the reaction was washed with ethanol and dispersed in 5 ml of ethanol to obtain Ag / Ag with a particle size of 50-60 nm and a shell thickness of 5-10 nm 2 S core / shell nanocrystalline dispersion colloid;
[0040] Take 50 microliters of colloid, in an area of about 0.5 × 0.5 cm 2 The aluminum sheet is spin-coated into a film, and then two films are used to assemble a resistance switch, and the I-V curve is measured, see Image 6 .
Example Embodiment
[0041] Example 3
[0042] In 50 ml of ethylene glycol, add 10 g of PVP (K30), magnetically stir, heat to 160 ℃, then add 0.5 g of silver nitrate, keep at 160 ℃ for 10 minutes; then, add 10 mg of sulfur powder to react at 160 ℃ For 10 minutes, the precipitate obtained from the reaction was washed with ethanol and dried at 40-80°C to obtain Ag / Ag with a particle size of 60-80 nm and a shell thickness of 2-5 nm. 2 S core / shell nanocrystals.
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