Quality control method of traditional Chinese medical preparation
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A quality control method and technology of traditional Chinese medicine preparations, applied in the direction of medical formula, non-central analgesics, antipyretics, etc., can solve the problems of no quality control method for juvenile fengdan, so as to promote product sales and improve controllability The effect of improvement of sex and quality standards
Active Publication Date: 2011-05-04
津药达仁堂集团股份有限公司达仁堂制药厂
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[0007]According to the search, there is currently no relevant patent on the quality control method of Baoyouhua
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[0059] Below in conjunction with the examples, the present invention is further described, the following examples are illustrative, not limiting, and the protection scope of the present invention cannot be limited by the following examples.
[0060] A kind of quality control method of traditional Chinese medicine preparation Baoyouhuafengdan, the steps of its method are:
[0061] (1) Microscopic identification:
[0062] The microscopic description is as follows: Since this product is raw powder used as medicine, the diameter of calcium oxalate cluster crystals is 20-68 μm, with sharp edges and corners; the parenchyma cells around the fiber bundles contain square crystals of calcium oxalate, forming crystal fibers; the thick-walled cells are polygonal or long polygonal , 70-180 μm in diameter, thick wall, slightly lignified, and obvious pits; hesperidin crystals are slightly yellowish, present in mesophyll tissue, especially in palisade cells; tubules contain brown-yellow secre...
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Abstract
The invention relates to a quality control method of a traditional Chinese medical preparation. The method comprises the following steps of: firstly, carrying out microscopic identification; secondly, identifying whether a juvenile wind-transmission pill prescription contains the contents of notopterygium root, radix sileris, rhizome of chuanxiong, ginseng and liquorice or not by adopting a film chromatography; and finally, measuring the liquorice content in the juvenile wind-transmission pill prescription by adopting a high-efficiency liquid-phase method and using ammonium glycyrrhetate as a reference substance. Based on an original standard of the traditional Chinese medical set prescription preparation volume III of the drug standard of the health department, the detection method provided by the invention adds the film identification detection methods of reference medical materials and reference substances and a method for measuring the content by using a high-efficiency liquid-phase chromatography. The revised quality standard control method improves the controllability of the juvenile wind-transmission pill quality standard, further ensures the internal quality and the curative effect of the product and is significant to promote the product marketing, enhance the market competitiveness of the product and ensure the drug safety for patients.
Description
technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and relates to a detection method of traditional Chinese medicines, in particular to a quality control method of the traditional Chinese medicine preparation Baoyouhuafengdan. Background technique [0002] Baoyouhuafengdan is composed of Dannanxing, Peppermint, Notopterygium, Duhuo, Tianma, Nepeta, Chuanxiong, Scorpion, Licorice, Ginseng, and Fangfeng. Its preparation method is: the above eleven ingredients are crushed into fine powder, and mixed , sieve, add 105-115g of refined honey for every 100g of powder, and make big honeyed pills, that is to say. Baoyou Huafeng Pill has the effect of clearing away heat and dispersing wind, relieving cough and resolving phlegm. It is used for convulsions with internal heat, excessive phlegm and salivation, cough and fever, headache and body pain, twitching of limbs, and restless sleep. [0003] With the continuous development of the e...
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