Method for improving dissolubility of wheat gluten by ultrasonic treatment
A technology of ultrasonic treatment and gluten powder, which is applied in the field of gluten powder processing, can solve the problems of large hydrophobic area, low solubility, and limited application range, etc., and achieve short modification time, low temperature requirements, and low energy consumption Effect
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Embodiment 1
[0023] Step 1, get 12g gluten powder (domestic), add 200ml deionized water, stir and hydrate at 25°C for 10 minutes to obtain gluten powder suspension.
[0024] Step 2, under the action of magnetic stirring, adjust the pH value of the gluten suspension to 4.5 with hydrochloric acid.
[0025] Step 3. Ultrasonic treatment is carried out on the suspension after adjusting the pH value. The ultrasonic equipment is a probe type, and the pulse amplitude is set to 50%. The ultrasonic treatment adopts intermittent operation. 10s, the ultrasonic process was carried out in an ice bath environment, and the ultrasonic time was 80s.
[0026] Step 4. Spray-dry the ultrasonically treated gluten powder dispersion, control the inlet temperature to 160° C., and the outlet temperature to 55° C., and pass the dried powder through a 100-200 mesh sieve to obtain modified gluten powder. The gluten powder after ultrasonic modification is light yellow powder with loose structure, uniform particles and...
Embodiment 2
[0028] Step 1, get 9g gluten powder (domestic), add 200ml deionized water, stir and hydrate at 25°C for 5 minutes to obtain gluten powder suspension.
[0029] Step 2, under the action of magnetic stirring, adjust the pH value of the gluten suspension to 3.5 with hydrochloric acid.
[0030] Step 3. Ultrasonic treatment is carried out on the suspension after adjusting the pH value. The ultrasonic equipment is a probe type, and the pulse amplitude is set to 40%. The ultrasonic treatment adopts intermittent operation. 1 s, the ultrasonic process was carried out in an ice bath environment, and the ultrasonic time was 60 s.
[0031] Step 4, spray-drying the ultrasonically treated gluten powder dispersion, controlling the inlet temperature to 180°C and the outlet temperature to 60°C, and passing the dried powder through a 100-200 mesh sieve to obtain modified gluten powder. The gluten powder after ultrasonic modification is light yellow powder with loose structure, uniform particles...
Embodiment 3
[0033] Step 1, get 20g gluten powder (domestic), add 200ml deionized water, stir and hydrate at 25°C for 30 minutes to obtain gluten powder suspension.
[0034] Step 2, under the action of magnetic stirring, adjust the pH value of the gluten suspension to 3 with hydrochloric acid.
[0035] Step 3. Ultrasonic treatment is carried out on the suspension after adjusting the pH value. The ultrasonic equipment is a probe type, and the pulse amplitude is set to 80%. The ultrasonic treatment adopts intermittent operation. 15s, the ultrasonic process was carried out in an ice bath environment, and the ultrasonic time was 120s.
[0036] Step 4, freeze-drying the gluten powder dispersion after ultrasonic treatment at a temperature of -45° C. for 24 hours, and passing the dried powder through a 100-200 mesh sieve to obtain modified gluten powder. The gluten powder after ultrasonic modification is light yellow powder with loose structure, uniform particles and no agglomeration.
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