Preparation process of loaded water-controlled sand with phase permeability regulating function
A technology of phase permeability and preparation process, which is applied in the field of load-type water-controlling sand preparation process, can solve problems such as energy waste, affecting oil well productivity, affecting development efficiency or economic benefits, etc., to reduce production costs, prolong stable production period, improve Effects on development efficiency or economics
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Embodiment 1
[0014] Step A) Cleaning the surface of quartz sand or ceramsite: Soak with 95% industrial ethanol and stir for 15 minutes, then place it at room temperature to dry.
[0015] Step B) is the surface modification method of quartz sand or ceramsite: put the required 1 quartz sand or ceramsite into the stirring tank, add an aqueous solution containing 1% volume of coupling agent KH-560, stir and slowly heat up to 80°C, so that The coupling agent undergoes a hydrolysis reaction on the surface of the quartz sand for 20 minutes.
[0016] Step C) is to mix the surface-modified quartz sand or ceramsite with a mixture of monomeric acrylic acid, propylene, sulfonated propylene and deionized water, and self-polymerize under the action of an initiator to form a load-type water-controlling material with a phase permeability adjustment function. Sand: a. Mix the quartz sand or ceramsite after the hydrolysis reaction in step B) with the mixture of monomer acrylic acid, propylene, sulfonated pr...
Embodiment 2
[0018] Step A) Cleaning the surface of quartz sand or ceramsite: Soak with 95% industrial ethanol and stir for 15 minutes, then place it at room temperature to dry.
[0019] Step B) is the surface modification method of quartz sand or ceramsite: put the required 1 quartz sand or ceramsite into the stirring tank, add an aqueous solution containing 2% by volume of coupling agent C-439, stir and slowly raise the temperature to 70°C to make the coupling The coupling agent undergoes hydrolysis reaction on the surface of quartz sand for 30 minutes.
[0020] Step C) is to mix the surface-modified quartz sand or ceramsite with a mixture of monomeric acrylic acid, propylene, sulfonated propylene and deionized water, and self-polymerize under the action of an initiator to form a load-type control compound with a phase permeability adjustment function. Water sand: a. Mix the quartz sand or ceramsite after the hydrolysis reaction in step B) with the mixture of monomer acrylic acid, propyl...
Embodiment 3
[0022] Step A) Cleaning the surface of quartz sand or ceramsite: Soak with 95% industrial ethanol and stir for 15 minutes, then place it at room temperature to dry.
[0023] Step B) is the surface modification method of quartz sand or ceramsite: put the required 1 quartz sand or ceramsite into the stirring tank, add an aqueous solution containing 3% volume of coupling agent A-143, stir and slowly heat up to 80°C, The coupling agent was hydrolyzed on the surface of the quartz sand for 40 minutes. The solid initiator is a mixture of sodium bisulfite and ammonium persulfate with a mass ratio of 1:2.
[0024] Step C) is to mix the surface-modified quartz sand or ceramsite with a mixture of monomeric acrylic acid, propylene, sulfonated propylene and deionized water, and self-polymerize under the action of an initiator to form a load-type control compound with a phase permeability adjustment function. Water sand: a. Mix the quartz sand or ceramsite after the hydrolysis reaction in ...
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