Cyclopropene preservative, and preparation and packaging methods thereof
A technology of propylene and antistaling agents, which is applied in the field of cyclopropene antistaling agents and its preparation, and can solve problems such as content decline and instability
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[0068] Example 1: Preparation of cyclopropene inclusion compound powder
[0069] The synthesized and purified 1-MCP gas is passed into a 10 kg absorption solution composed of 14.5% α-cyclodextrin, 5% white carbon black and 80.5% water, and performs inclusion absorption at room temperature. The stirring speed is 300 revolutions per minute, continue to infuse 1-MCP gas for 3 hours, then quickly suction filter the absorption liquid mixture, add absolute ethanol to rinse after suction filtration, then suction filter, and finally dry at room temperature to obtain 1.9 kg containing 3.0 % 1-methylcyclopropene inclusion compound powder.
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[0070] Example 2: Preparation of cyclopropene inclusion compound powder
[0071] The synthesized and purified 1-MCP gas is passed into 10 kilograms of absorption solution composed of 1% alkylated α-cyclodextrin, 49% white carbon black, and 50% water, and then undergoes inclusion absorption at room temperature. The stirring speed is 300 revolutions per minute, and 1-MCP gas is continuously introduced for 5 hours. Then the absorption liquid mixture is subjected to rapid suction filtration. After the suction filtration is completed, anhydrous ethanol is added for washing, and then suction filtration, and drying at room temperature to obtain 4.95 kg Contains 0.07% 1-methylcyclopropene inclusion compound powder.
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[0072] Example 3: Preparation of cyclopropene inclusion compound powder
[0073] The synthesized and purified 1-MCP gas is passed into 10 kg of absorption liquid composed of 49% esterified α-cyclodextrin, 0.1% white carbon black and 50.9% water, and then undergoes inclusion absorption at room temperature and stirring The speed is 300 revolutions per minute, the 1-MCP gas is continuously introduced for 2 hours, and then the absorption liquid mixture is subjected to rapid suction filtration. After the suction filtration is completed, anhydrous ethanol is added for washing, and then suction filtration. After drying at room temperature, 5 kg 3.2% 1-methylcyclopropene inclusion compound powder.
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