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A suitable ion source for time-of-flight mass spectrometer

A technology of time-of-flight mass spectrometry and ion source, which is applied in the field of ion source and extraction device, can solve the problems of low ion utilization rate, restricted instrument sensitivity, etc., and achieve the effects of improving sensitivity, increasing ion extraction efficiency, and improving utilization rate.

Inactive Publication Date: 2011-12-21
XIAMEN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the ion source delivers a continuous ion flow, it will cause the ions to enter the time-of-flight mass spectrometer only when there is a pulse voltage, so the utilization rate of the ions is very low (<10%), and the sensitivity of the instrument is also affected. Great constraints

Method used

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  • A suitable ion source for time-of-flight mass spectrometer
  • A suitable ion source for time-of-flight mass spectrometer
  • A suitable ion source for time-of-flight mass spectrometer

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Embodiment Construction

[0023] The present invention will be further described below with reference to the drawings and embodiments.

[0024] See figure 1 , The embodiment of the present invention is provided with a sample injection booster pump 1, a solenoid valve 2, a repelling electrode 3 (sheet shape), an ionization chamber 4 (square), an intermediate grid 6, an extraction grid 7, a focusing electrode 8 (cylinder Shape), exit pole piece 9 (sheet shape) and filament 5 (tungsten wire).

[0025] The inlet of the injection booster pump 1 is the sample inlet, the outlet of the injection booster pump 1 is connected with the inlet of the solenoid valve 2, the outlet of the solenoid valve 2 is connected with the inlet of the repelling electrode 3, and the repelling electrode 3 is arranged at the inlet of the ionization chamber 4 Inside, the middle grid 6 is arranged at the outlet end of the ionization chamber 4, the extraction grid 7 is arranged on the side of the intermediate grid 6, the focusing electrode 8...

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Abstract

The invention discloses an ion source suitable for a flight time mass spectrometer, which relates to an ion source for a mass spectrometer. The ion source is provided with a sample introduction booster pump, a solenoid valve, a repulsion electrode, an ionization chamber, a middle grid, an extraction grid, a focusing electrode, an emergent pole piece and an excitation source generator, wherein theoutlet of the sample introduction booster pump is communicated with the inlet of the solenoid valve; the outlet of the solenoid valve is communicated with the inlet of the repulsion electrode; the repulsion electrode is arranged in the inlet end of the ionization chamber; the middle grid is arranged at the outlet end of the ionization chamber; the extraction grid is arranged at the side of the middle grid; the focusing electrode and the emergent pole piece are successively arranged at the side of the extraction grid; the focusing electrode and the emergent pole piece are both provided with a central ion extraction through hole; the ionization chamber, the repulsion electrode, the middle grid, the extraction grid, the focusing electrode and the emergent pole piece are coaxial; a filament is arranged out of the upper end and the lower end of the ionization chamber; and the excitation source generator faces to an energy beam incidence hole arranged on the ionization chamber. According tothe ion source, a pulse ion group can be generated, the ion extraction efficiency is greatly improved, the ion use ratio is improved, and the sensitivity of the mass spectrometer is improved.

Description

Technical field [0001] The invention relates to an ion source of a mass spectrometer, in particular to an ion source and extraction device of a time-of-flight mass spectrometer. Background technique [0002] The mass spectrometer is one of the most important members in the field of modern scientific analytical instruments, and one of the most advanced means of modern analytical science. The mass spectrometer is a modern precision analytical instrument that first ionizes the sample, and then passes through a preset electric or magnetic field to achieve mass-to-charge ratio separation, and detects the corresponding peak intensity, so as to achieve qualitative and quantitative analysis of the sample. From the initial isotope analysis, mass spectrometry has gradually become an indispensable analysis and detection method in many aspects such as chemistry, geology, biochemistry, pharmacology, medicine, petrochemical industry, energy, environmental protection and food processing. [0003...

Claims

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Application Information

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IPC IPC(8): H01J49/14H01J49/06
Inventor 何坚
Owner XIAMEN UNIV
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