Electrocoating composition and method for electrocoating
A coating method and composition technology, applied in electrolytic coatings, electrophoretic coatings, epoxy resin coatings, etc., can solve problems such as undesired coagulant effects
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[0066] The content of the present invention will be specifically described below with reference to Examples and Comparative Examples.
[0067] In the examples, "parts" and "%" are based on weight unless otherwise indicated.
[0068] Synthesis of Cationic Epoxy Resin
[0069] In the flask equipped with stirrer, cooling pipe, nitrogen introduction pipe, thermometer and dropping funnel, add 92 parts of 2,4- / 2,6-toluene diisocyanate (weight ratio=8 / 2), 95 parts of formaldehyde methyl isobutyl ketone (hereinafter referred to as MIBK) and 0.5 parts of dibutyltin dilaurate. While stirring the reaction mixture, 21 parts of methanol were added dropwise. The reaction started at room temperature and was exothermic to 60°C.
[0070] Thereafter, after continuing the reaction for 30 minutes, 57 parts of ethylene glycol mono-2-ethylhexyl ether were dropped from the dropping funnel. Next, 42 parts of bisphenol A-propylene oxide 5-mol adducts were added to the reaction mixture. The reacti...
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