Phosphorus-free, fluorine-free and heavy metal-free phosphorus displacing agent and preparation method thereof
A technology of heavy metal and phosphorus replacement agent, applied in the direction of metal material coating process, etc., can solve problems such as environmental pollution, and achieve the effects of low comprehensive cost, uniform film formation, and strong anti-corrosion performance.
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[0025] Embodiment: the preparation method of phosphorus-free, fluorine-free and heavy-metal-free phosphoreplacement agent comprises the following steps:
[0026] a. Preparation: Salt: 100 grams of magnesium nitrate, 120 grams of sodium gluconate, 12 grams of sodium tungstate, 50 grams of disodium EDTA; acid: 60 grams of nitric acid, 40 grams of gluconic acid; alkali: 10 grams of caustic soda;
[0027] b. Preparation of shielding agent: first take 100 grams of tap water and add it to a stainless steel reaction kettle, heat it to 60-80 ° C, slowly add 50 grams of disodium EDTA to dissolve, cool down after the dissolution, and then slowly add 20 grams of EDTA Gluconic acid is cooled for subsequent use after the reaction is completed;
[0028] c. Preparation of additives: take 80 grams of tap water and add it to a stainless steel reactor, heat it to 70-90 ° C, slowly add 20 grams of gluconic acid, and then slowly add 12 grams of sodium tungstate after dissolution, and keep stirr...
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